Fabrication of Toughened Alumina Nanocomposites Using γ-Alumina Powder

Article Preview

Abstract:

To improve fracture strength and fracture toughness in ceramic materials, we focused our attention on an intra-type structure of nanocomposites. We proposed new processing method for fabricating intra-type nanocomposites. In this work, Al2O3/Ni nanocomposites were fabricated using a soaking method and sintered by PECS(Pulse Electric Current Sintering) method. We also estimated seed effects on this system. Seeded nanocomposites showed high fracture strength and higher fracture toughness than non-seeded nanocomposites and monolithic alumina. The fracture strength of the seeded nanocomposites was more than 800MPa in all sintering temperature range. The maximum value of the fracture toughness was 5.5 MPa⋅m1/2 for the specimen sintered at 1350°C. The sintered specimens with high fracture strength and high fracture toughness were annealed from 800°C to 1000°C for 0 to 10 min. The specimen annealed at 800°C for 5 min showed the highest fracture toughness of 7.6 MPa⋅m1/2. This value is two times higher than that of the monolithic alumina.

You might also be interested in these eBooks

Info:

Periodical:

Advanced Materials Research (Volumes 11-12)

Pages:

583-586

Citation:

Online since:

February 2006

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2006 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] B. Harris, S.E. Dorey and R.G. Cooke: Composite. Sci. Tech. Vol. 31 (1988), p.121.

Google Scholar

[2] W.J. Clegg, K. Kendfall, N. McN. Alford and J.D. Birchall: Nature Vol. 347 (1990), p.455.

Google Scholar

[3] K. Niihara: J. Ceram. Soc. Jpn. Vol. 99 (1991), p.974.

Google Scholar

[4] H. Awaji, S-M. Choi and E. Yagi: Mech. Mater. Vol. 34 (2002), p.411.

Google Scholar

[5] S-M. Choi and H. Awaji: Sci. Tech. Adv. Mater. Vol. 6 (2005), p.2.

Google Scholar

[6] H. Awaji and Y. Sakaida: J. Am. Ceram. Soc. Vol. 73 (1990), p.3522. 0 5 10.

Google Scholar

[8] 0 Fracture toughness /MPam 1/2 Annealing time / min 0 5 10.

Google Scholar

[8] 0 � before annealing � annealed at 800 � � annealed at 900 � � annealed at 1000 � Fracture toughness /MPam 1/2 Fracture toughness /MPam 1/2 Annealing time / min 0 5 10.

Google Scholar

[8] 0 Fracture toughness /MPam 1/2 Fracture toughness /MPam 1/2 Annealing time / min 0 5 10.

Google Scholar

[8] 0 � before annealing � annealed at 800 � � annealed at 900 � � annealed at 1000 � � before annealing � annealed at 800 � � annealed at 900 � � annealed at 1000 � Fracture toughness /MPam 1/2 Fracture toughness /MPam 1/2 Annealing time / min Fig. 6. Fracture toughness of Al2O3/Ni nanocomposites annealed at various conditions. 1200 1300 1400 1500 1600 2 3 4 5 Fracture toughness / MPam 1/2 Sintering temperature / � Fig. 5. Fracture toughness of sintered Al2O3/Ni nanocomposites. � non-seed nanocomposites � seeded nanocomposites � monolithic alumina.

DOI: 10.4271/ams5867b

Google Scholar