Comparison between Different LiFePO4 Synthesis Routes

D. Jugović; N. Cvjetićanin; M. Mitrić; S. Mentus

doi:10.4028/www.scientific.net/MSF.555.225

Paper Titles

Investigation of (PO₄)/(WO₆)₃ - Lattice Components of Keggin`s Anion Interaction with Cations in Alkaline-Earth Salts of 12-Tungstophosphoric Acid
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Characterization of Insoluble Monovalent K⁺, Tl⁺ and Ag⁺ Salts of 12-Tungstophosphoric Acid
p.207

The Activity of Iron-Containing Zeolitic Materials for the Catalytic Oxidation in Aqueous Solutions
p.213

Structural Investigation of Ba²⁺ and Sr²⁺ Diphyllosilicates Doped with Yb³⁺ Ions
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Comparison between Different LiFePO₄ Synthesis Routes
p.225

Rietveld Refinement of Crystal Phases (Ca_1-xLa_x)MnO₃ with Perovskite-Type Structure
p.231

Synthesis of Pure and Doped LaMnO₃ Powders from Citrate Precursors
p.237

Raman Spectra of Bismuth Titanate Ceramics
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Dielectric and Ferroelectric Properties of BaTi_1-xSn_xO₃ Multilayered Ceramics
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HomeMaterials Science ForumMaterials Science Forum Vol. 555Comparison between Different LiFePO4 Synthesis...

Comparison between Different LiFePO₄ Synthesis Routes

Abstract:

Olivine-type lithium iron phosphate (LiFePO4) powders were synthesized applying three different methods: solid state reaction at high temperature, ultrasonic spray pyrolysis, and sonochemical treatment. The samples were characterized by X-ray powder diffraction (XRPD). Particle morphologies of the obtained powders were determined by scanning electron microscopy (SEM). It was found that structural and microstructural parameters of this material were strongly dependent on the synthesis conditions. We present here the results obtained upon optimization of each procedure for designing this cathode material.

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Materials Science Forum (Volume 555)

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225-230

DOI:

https://doi.org/10.4028/www.scientific.net/MSF.555.225

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Online since:

September 2007

Authors:

D. Jugović, N. Cvjetićanin, M. Mitrić, S. Mentus

Keywords:

Cathode Material, LiFePO₄/C, Refinement, Sonochemistry, Ultrasonic Spray Pyrolysis

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