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Mapping of Composition, Phase Transitions and Properties in Oxidized Ti3SiC2
Abstract:
The oxidation characteristics, composition profile and phase transition of Ti3SiC2 in the temperature range 20-1400°C have been investigated by in-situ neutron diffraction and secondary ion mass spectroscopy (SIMS). Anatase has been observed to form at ~600°C, rutile at ~750°C and cristobalite at ∼1300°C. Depth-profiling results by SIMS and Vickers indentation have revealed a distinct gradient in composition and microhardness within the surface oxide layers.
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986-988
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February 2008
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© 2008 Trans Tech Publications Ltd. All Rights Reserved
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