Paper Title:
Direct Deoxidation of ZrOCl2 Powder to Zirconium With Non-Sintering
  Abstract

Direct electro-deoxidation of zirconium oxychloride powder without sintering in molten CaCl2 and NaCl mixture salt was studied. Molten CaCl2 and NaCl mixture salt as electrolyte, a little graphite crucible filled with zirconium oxychloride powder as novel cathode and a graphite rod as anode, deoxidation experiments were performed at 700 and 3.2V for 8h and 15h, respectively. Results show that using new material of zirconium oxychloride and the method of direct electro-deoxidation without sintering can be applied to the preparation of fine zirconium metal particles, which have a great advantage in cheap cost, short technical process, and energy saving.

  Info
Periodical
Advanced Materials Research (Volumes 146-147)
Edited by
Sihai Jiao, Zhengyi Jiang and Jinglong Bu
Pages
775-779
DOI
10.4028/www.scientific.net/AMR.146-147.775
Citation
X. Y. Zou, H. W. Xie, Y. C. Zhai, X. C. Lang, "Direct Deoxidation of ZrOCl2 Powder to Zirconium With Non-Sintering", Advanced Materials Research, Vols. 146-147, pp. 775-779, 2011
Online since
October 2010
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