Paper Title:
Foundation of the Standard Curve Database for Quantitative Analysis by Internal Standard Method Based on XRD
  Abstract

In order to make quantitative analysis by internal standard method, 24 standard curves of inorganic compounds including quartz, corundum, TiO2, BaTiO3, etc. were obtained and the corresponding quantitative analyses were accomplished based on the quantitative analysis software attached in Rigaku D/Max-2200 X-Ray diffractometer. Results show that the coefficient of association R of the as-prepared curves are at the range of 0.928-0.980. By validating the samples with due content, it reveals that the analytical results are consistent with the actual values well, which indicate that the prepared standard curves are suitable for high-precision XRD phase quantitative analysis. Uniformity of samples is an important factor in the quantitative analysis by internal standard method.

  Info
Periodical
Edited by
Yiwang Bao, Li Tian and Jianghong Gong
Pages
1-4
DOI
10.4028/www.scientific.net/AMR.177.1
Citation
J. P. Wu, C. Y. Yao, L. Y. Cao, J. F. Huang, H. Y. He, H. Zhu, "Foundation of the Standard Curve Database for Quantitative Analysis by Internal Standard Method Based on XRD", Advanced Materials Research, Vol. 177, pp. 1-4, 2011
Online since
December 2010
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