Paper Title:
Hydrothermal Preparation and Formation Mechanism of ZnSn(OH)6 Cubic Aggregates and Zn2SnO4 Octahedra
  Abstract

ZnSn(OH)6 hierarchical cubes and Zn2SnO4 octahedra have been synthesized through a rapid, template-free, one-pot hydrothermal approach using zinc acetate, tin chloride and sodium hydroxide. ZnSn(OH)6 aggregates with cubic morphology and uniform size distribution have been successfully synthesized via aggregation-mediated crystallization. Through adjusting the hydrothermal parameters, Zn2SnO4 octahedra were obtained at a higher temperature. The formation of Zn2SnO4 octahedra undergone a transformation from ZnSn(OH)6 cubes. The as-synthesized products were characterized by powder X-ray diffraction (XRD), scanning electron microscopy (SEM) and differential scanning calorimetric analysis (DSC) and thermogravimetric analysis (TG).

  Info
Periodical
Advanced Materials Research (Volumes 194-196)
Edited by
Jianmin Zeng, Taosen Li, Shaojian Ma, Zhengyi Jiang and Daoguo Yang
Pages
693-699
DOI
10.4028/www.scientific.net/AMR.194-196.693
Citation
L. X. Yang, J. Y. Liu, P. J. Zhang, Y. X. Yang, P. Yin, X. P. Jiang, L. F. Qin, Y. Y. Tang, "Hydrothermal Preparation and Formation Mechanism of ZnSn(OH)6 Cubic Aggregates and Zn2SnO4 Octahedra", Advanced Materials Research, Vols. 194-196, pp. 693-699, 2011
Online since
February 2011
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Price
$32.00
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