Paper Title:
Low-Pressure Preheating Combustion Synthesis of Silicon Nitride
  Abstract

Silicon nitride was prepared by means of low-pressure preheating combustion synthesis in this paper. When N2 pressure is less than or equal to 2MPa, the lowest preheating temperature is about 653K, reactant could make silicon nitride by combustion synthesis. The additive of ammonium fluoride and ammonium chloride, as the reactive diluent, and Si react and make some useful intermediate products to α -Si3N4 after thermal decomposition. The reactive diluent content must be appropriate. At the same time, with the improvement of Si3N4, as the inert diluent, content in reactant, the adiabatic flame temperature of system would reduce, and combustion reaction rate of Si also drops, so it is propitious to make high level of α -Si3N4.

  Info
Periodical
Advanced Materials Research (Volumes 26-28)
Edited by
Young Won Chang, Nack J. Kim and Chong Soo Lee
Pages
441-444
DOI
10.4028/www.scientific.net/AMR.26-28.441
Citation
K. Zhang, L. Bai, W. P. Shen, C. C. Ge, "Low-Pressure Preheating Combustion Synthesis of Silicon Nitride", Advanced Materials Research, Vols. 26-28, pp. 441-444, 2007
Online since
October 2007
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Price
$32.00
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