Paper Title:
Preparation of (Mo,Nb)Si2 Ternary Alloys by Self−Propagating High−Temperature Synthesis
  Abstract

An experimental study on the preparation of (Mo,Nb)Si2 ternary alloys was conducted by self-propagating high-temperature synthesis method from elemental powder compacts of different stoichiometries. And the combustion mode, combustion temperature, flame-front propagation velocity and product structure were discussed. The results show that (Mo,Nb)Si2 ternary alloys are characterized by an unsteady state combustion mode with a spiral−trajectory reaction front from top to bottom. The combustion temperature and flame−front propagation velocity decrease with the addition of coarse niobium powder. The combustion temperature and flame-front propagation velocity of MoSi2 are 1629K and 3.13mm/s respectively. However, those of (Mo0.8Nb0.2)Si2 alloy are 1460K and 1.97mm/s. The solid solubility of niobium in MoSi2 is less than 2.5at.%, and the combustion synthesis produce still remains Cllb single-phase structure in (Mo1-x,Nbx)Si2(x<0.075) sample. The C40-type structure appears in (Mo0.925,Nb0.075)Si2 compact and the intensity of diffraction peaks of C40-type phase gradually reinforces with the increase of niobium content. Combustion synthesis is an effective technology for producing (Mo,Nb)Si2 ternary alloys.

  Info
Periodical
Edited by
Deliang Chen
Pages
219-222
DOI
10.4028/www.scientific.net/AMR.266.219
Citation
P. Z. Feng, S. Zhang, X. H. Wang, W. S. Liu, J. Wu, "Preparation of (Mo,Nb)Si2 Ternary Alloys by Self−Propagating High−Temperature Synthesis", Advanced Materials Research, Vol. 266, pp. 219-222, 2011
Online since
June 2011
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