The bulk metallic glass has received much attention from scientist and engineer. In this paper, we fabricated metallic glass of Nd-based and carried out experimental research. This kind of metallic glass has shown a distinct glass transition and stable super-cooled liquid region. At the same time, we find the paramagnetic performance of Nd-based metallic glass is different from other hard magnetic alloys at ordinary temperature. The DSC experiment indicate that the glass transition temperature increase with the heating temperature.