Paper Title:
Research of Catalytic Oxidation Synthesis of Cyclopentene to Glutaraldehyde
| Periodical | Advanced Materials Research (Volumes 391 - 392) |
|---|---|
| Main Theme | Chemical Engineering and Material Properties |
| Edited by | H.M. Zhang and B. Wu |
| Pages | 1149-1152 |
| DOI | 10.4028/www.scientific.net/AMR.391-392.1149 |
| Citation | Qi Dong Yan et al., 2011, Advanced Materials Research, 391-392, 1149 |
| Online since | December, 2011 |
| Authors | Qi Dong Yan, Jun Xu, Feng Xu |
| Keywords | Catalysis, Cyclopentene, Oxidation, Qlutaraldehyde, Tungstenic Acid-Boron Anhydride |
| Price | US$ 28,- |
View full size
Abstract
The paper has studied the process of using H2O2 as oxidant and tungsten acid as catalyst, catalytic oxidation synthesis process of cyclopentene to glutaraldehyde and explored the main influence factors of the reaction, including the reaction time, reaction temperature, catalyst dosage and solvent. Furthermore, the quantitative analysis and qualitative analysis of the product was characterized by gas chromatography. The optimum synthetic condition was as follows: tertiary butanol as solvent, tungsten acid: boron anhydride(mass ratio)=1:1, 30%H2O2 as oxidant, the reaction temperature 35℃, the reaction time 4h, the yield of glutaraldehyde yield was 46%.
