The Study of Purifying Coumarin Chemical Compounds in “Yubaizhi” Angelica Dahurica by Macro-Porous Absorption Resin
| Periodical | Advanced Materials Research (Volumes 468 - 471) |
|---|---|
| Main Theme | Automation Equipment and Systems |
| Edited by | Wenzhe Chen, Pinqiang Dai, Yonglu Chen, Dingning Chen and Zhengyi Jiang |
| Pages | 3060-3064 |
| DOI | 10.4028/www.scientific.net/AMR.468-471.3060 |
| Citation | Yan Long Wang et al., 2012, Advanced Materials Research, 468-471, 3060 |
| Online since | February, 2012 |
| Authors | Yan Long Wang, Hao Guo Tang, Mi Mi Guo |
| Keywords | Angelica Dahurica (Fisch. Ex Hoffim.)Benth.et Hook.f, Imperatorin, Isoimperatorin, Macro-Porous Absorption Resin, Purification, Yubaizhi |
| Price | US$ 28,- |
The method of using macro-porous absorption resin to rurify coumarins in “Yubaizhi” angelica dahurica was used in this study. A kind of better resin was chosen from D-101 resin and HPD600 resin by the comparison of adsorption rate, desorption rate and purity. The result showed that D-101 resin was better for purifying coumrins. Then these conditions of purifying were discussed. when the sample concentration was 0.1g medicinal materials per milliliter and the adsorbent speed was 1ml/min, the effect of adsorption was better. And per gram resin could adsorb coumarins of 3g sample material. When the eluotropic speed of 80% ethanol was 1ml/min and the dosage of eluent reaches was 7 multiple of bed volume, the effect of elution was better. The result of demonstration test showed the effect of purifying coumarin was better with above-mentioned conditions.