Paper Title:
In Air Synthesis of Bi2S3 and PbS Microcrystals by Thermolysis of Single-Source Precursors
  Abstract

Without the protection of inert gases or vacuum environment, rod-like Bi2S3 and cubic-shaped PbS microcrystals were synthesized directly via pyrolyzing corresponding metal diethyldithiocarbamates in air at 300 °C for 3 h. The products have been characterized by X-ray diffraction and scanning electron microscope, and their possible formation mechanisms were also tentatively proposed. Furthermore, control experiments with multiple-source precursors revealed that our single-source precursors played an important role in preparing phase-pure Bi2S3 and PbS.

  Info
Periodical
Advanced Materials Research (Volumes 79-82)
Edited by
Yansheng Yin and Xin Wang
Pages
1343-1346
DOI
10.4028/www.scientific.net/AMR.79-82.1343
Citation
Z. N. Du, Y. C. Zhang, "In Air Synthesis of Bi2S3 and PbS Microcrystals by Thermolysis of Single-Source Precursors", Advanced Materials Research, Vols. 79-82, pp. 1343-1346, 2009
Online since
August 2009
Export
Price
$32.00
Share

In order to see related information, you need to Login.

In order to see related information, you need to Login.

Authors: Renato Luiz Siqueira, Luiz Claudio Pardini, Inez Valéria Pagotto Yoshida, Marco Antônio Schiavon
Abstract:This work reports the synthesis and thermal characterization of poly(borosiloxanes) (PBS) derived from methyltrietoxysilane (MTES) and...
182
Authors: M. Ambika, R. Saravanan
Abstract: In this work, lead sulphide has been characterized using X- ray diffraction, SEM, EDX and UV-Visible techniques. X-ray analysis is...
153
Authors: A.S. Obaid, M.A. Mahdi, Asmiet Ramizy, Z. Hassan
Abstract:Nanocrystalline PbS thin films were prepared using chemical bath deposition method on glass substrates, together with lead acetate as a...
60
Authors: Peng Wang, Li Bo Fan, Li Juan Sun, Zhen Hua Zhang, Xin Bing Zhu, Yan Ge Zhang, Pin Jiang Li
Chapter 2: Materials Engineering
Abstract:A film solar cell was made with a structure of Glass/ITO/CdS/PbS/Al. CdS film was obtained by thermal evaporation. PbS film was prepared by a...
176