Paper Title:
Studies on Synthesis, Morphology and Theoretical Analysis of Schiff Base Derived From p-Aminobenzoic Acid and p-Hydroxybenzaldehyde by Solvent-Free Reaction Using Jet Milling
  Abstract

A novel synthesis method on solvent-free reaction using improved jet milling was described. Synthesis of a schiff base derived from p-hydroxybenzaldehyde and p-aminobenzoic acid had been achieved by solvent-free reaction using improved jet milling, and the structure of the compound have been characterized by Fourier transform infrared spectrometer, 1H nuclear magnetic resonance techniques and mass spectrometry. Differential thermal analysis of reaction process shown that the reaction was complete within 6 min. The scanning electron microscopy shown that the particles of the schiff base were regular and the size of the most particles was 0.5~1 μm. At the same time, the theoretical analysis about reaction process of solvent-free reaction using improved jet milling was preliminary studied. This solvent-free reaction using improved jet milling not only involves mild conditions, a simple operation and short reaction time, but also gives quantitative yield without waste producing work-up procedures. Simultaneously, the investigation also showed this reaction method was feasible, and of benefit to environment.

  Info
Periodical
Advanced Materials Research (Volumes 79-82)
Edited by
Yansheng Yin and Xin Wang
Pages
1355-1358
DOI
10.4028/www.scientific.net/AMR.79-82.1355
Citation
Y. H. Cai, "Studies on Synthesis, Morphology and Theoretical Analysis of Schiff Base Derived From p-Aminobenzoic Acid and p-Hydroxybenzaldehyde by Solvent-Free Reaction Using Jet Milling ", Advanced Materials Research, Vols. 79-82, pp. 1355-1358, 2009
Online since
August 2009
Authors
Export
Price
$32.00
Share

In order to see related information, you need to Login.

In order to see related information, you need to Login.

Authors: Li Yang, Wie Sheng Guan, Bo Bai, Yun Xiang
Abstract:A novel route for synthesis of biomorphic nickel oxide (NiO) hollow microspheres, using yeasts as bio-templates, has been successfully...
1867
Authors: Li Min Dong, Yan Li Zhuang, Zhi Dong Han, Ze Wu, Xian You Zhang
Abstract:Green phosphor of La(BO3, PO4): Ce, Tb was synthesized by means of sol-gel method and conventional solid state method. The thermal formation...
359
Authors: S. Alamolhoda, Saeed Heshmati-Manesh, Abolghasem Ataie, A. Badiei
Abstract:In this paper, effect of AlCl3 addition as process control agent (PCA) during high energy ball milling of Al and TiO2 powder mixture was...
626
Authors: Yi Shan Jiang, Jiang Hua Luo, Zhen Li, Lu Ning Chen
Chapter 9: Nano Materials
Abstract:Cornstalk fibers were modified with surface modification and the properties of cornstalk fiber/gypsum composites was studied. The results...
1162
Authors: X.J. Wang, X.C. Zhou
Chapter 2: Advanced Material and Manufacturing Technologies
Abstract:A novel material synthesis technique, microwave process was investigated for the production of phosphor powders. In this study, we have...
106