Paper Title:
Hydrothermal Synthesis and Characterization of Nanocrystalline Anatase Titania from Ti(OC4H9)4
  Abstract

Titania powders consisting of well-crystallized nanosize anatase phase were prepared by the hydrothermal synthesis from Ti(OC4H9)4 at T=568K and P=15.5MPa in the presence of C2H5OH and CO(NH2)2. DTA-TG, XRD and TEM were employed to characterize the samples. The results show that the crystallization temperature of the well-crystallized nanosize anatase phase to rutile is about 1123K, the particles distribute from 10nm to 50nm and it’s average diameter is about 30nm.

  Info
Periodical
Advanced Materials Research (Volumes 79-82)
Edited by
Yansheng Yin and Xin Wang
Pages
465-468
DOI
10.4028/www.scientific.net/AMR.79-82.465
Citation
R. J. Gao, P. W. Wu, "Hydrothermal Synthesis and Characterization of Nanocrystalline Anatase Titania from Ti(OC4H9)4", Advanced Materials Research, Vols. 79-82, pp. 465-468, 2009
Online since
August 2009
Export
Price
$32.00
Share

In order to see related information, you need to Login.

In order to see related information, you need to Login.

Authors: Maria Zaharescu, Maria Preda, Maria Crışan, Victor Fruth, S. Preda
143
Authors: D.L. Morgan, E.R. Waclawik, R.L Frost
Abstract:Nanotubes were produced from commercial and self-prepared anatase and rutile which were treated with 7.5 M NaOH over a temperature range of...
211
Authors: Ze Hua Zhou, Wen Kui Li, Zhi Qin Chen
Abstract:Nanocrystalline titanium dioxide was synthesized by microwave hydrothermal (MH) using tetrabutyl titanate and normal butyl alcohol as start...
1461
Authors: Xi Xin Wang, Jian Ling Zhao, Zhao Hui Meng, Jia Wei Yan
Abstract:Titania nanoparticles were successfully synthesized through an easily controlled and simple autothermal gelation process. Effects of H2O2...
1188
Authors: Lin Li, Sheng Qi Xi, Yang Nan Xing, Fei Hu Shang
Abstract:Titania powder was prepared by a sol-gel method and heat-treatment (HT). The morphology and structure of the titania powder were...
849