The Synthesis and Characterization of ZrW2O7(OH1-X,ClX)2·2H20 (X=0.016, 0.025) |
|
| Journal | Defect and Diffusion Forum (Volumes 251 - 252) |
|---|---|
| Volume | Defects and Diffusion Ceramics Abstracts |
| Edited by | David J. Fisher |
| Pages | 21-26 |
| DOI | 10.4028/www.scientific.net/DDF.251-252.21 |
| Citation | Yi Long Cao et al., 2006, Defect and Diffusion Forum, 251-252, 21 |
| Online since | March, 2006 |
| Authors | Yi Long Cao, Xue Bin Deng, Hui Ma, Shui Feng Wang, Xin Hua Zhao |
| Keywords | Acid Steam Hydrothermal (ASH), Chlorine Measurement, Structure Refinement, ZrW2O7(OH1-X,ClX)2·2H2O |
| Abstract | ZrW2O7(OH1-x,Clx)2·2H2O (x = 0.016, 0.025) is prepared by using the acid steam hydrothermal (ASH) method. The chlorine contents of the crystals are measured by means of potentiometric titration and ICP, respectively. The as-prepared powders are characterized by X-ray diffraction, and their structures are refined by using the Rietveld method contained in the GSAS program. The results indicate that the chloride ion occupies the hydroxyl group crystal site statistically. |
| Full Paper | 
Get the full paper by clicking here
|
First page example
