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A Rapid Setting TTCP-DCPD Cement. Study of the Setting Reaction as a Function of Time

Journal Key Engineering Materials (Volumes 284 - 286)
Volume Bioceramics 17
Edited by Panjian Li, Kai Zhang and Clifford W. Colwell, Jr.
Pages 15-18
DOI 10.4028/www.scientific.net/KEM.284-286.15
Citation E.F. Burguera et al., 2005, Key Engineering Materials, 284-286, 15
Online since April, 2005
Authors E.F. Burguera, Francisco Guitián, Laurence C. Chow
Keywords Calcium Phosphate Cement (CPC), Compressive Strength, Dicalcium Phosphate Dihydrate, Hydroxyapatite Formation, Setting Reaction, Tetracalcium Phosphate
Abstract

The progression of the setting reaction of a tetracalcium phosphate (TTCP) –dicalcium phosphate dihydrate (DCPD) rapid setting cement was investigated as a function of time. Compressive strength and extent of conversion to hydroxyapatite (HA) were obtained at different incubation times. The results indicated a rapid development of both strength and HA conversion in the early stages of the reaction, which slowed down after 4 h, presumably as a result of HA formation on the surface of the reactants. This hypothesis was supported by scanning electron microscopy examination of cement fracture surfaces.

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