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A Method for Simultaneously Precipitating and Dispersing Nano-Sized Calcium Phosphate Suspensions

Journal Key Engineering Materials (Volumes 284 - 286)
Volume Bioceramics 17
Edited by Panjian Li, Kai Zhang and Clifford W. Colwell, Jr.
Pages 67-70
DOI 10.4028/www.scientific.net/KEM.284-286.67
Citation A.F. Lemos et al., 2005, Key Engineering Materials, 284-286, 67
Online since April, 2005
Authors A.F. Lemos, A.H.S. Rebelo, J.H.G. Rocha, José Maria F. Ferreira
Keywords Calcium Phosphate, Colloidal Processing, Precipitation, Rheology
Abstract

Stable and relatively concentrated aqueous suspensions of nano-sized stoichiometric hydroxyapatite could be prepared by a precipitation method in the presence of suitable surface active agent (SAA). The method includes the precipitation, vacuum filtration and washing of the precipitated powders, followed by re-dispersion. It could be concluded that the added amount of the SAA should be enough to cover the primary particles surface, and that washing should be better carried out using a SAA solution. The method developed enables the precipitation of the powders and the preparation of suspensions, while significantly shortening the overall time required for colloidal processing consuming.

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