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Nano-Indentation of SiC and Si3N4/SiC Ceramic Materials

Journal Key Engineering Materials (Volume 290)
Volume Fractography of Advanced Ceramics II
Edited by J. Dusza, R. Danzer and R. Morrell
Pages 272-275
DOI 10.4028/www.scientific.net/KEM.290.272
Citation Miroslav Balog et al., 2005, Key Engineering Materials, 290, 272
Online since July, 2005
Authors Miroslav Balog, Pavol Šajgalík, Zoltán Lenčéš, Miroslav Hnatko, Jozef Kečkéš, Jow Lay Huang, J. Janega, R. Horváthová
Keywords Hardness, Modulus, Nanoindentation, Silicon Carbide (SiC)
Abstract

The present paper deals with the nano-indentation of SiC-micro and Si3N4/SiCmicro/ nano ceramic materials. The investigated SiC-micro and Si3N4/SiC-micro/nano ceramics were prepared by liquid phase sintering. Liquid phase was formed from different sintering additives (Y2O3, Yb2O3, Sm2O3). In the case of Si3N4/SiC-micro/nano ceramics the SiC nano-grains were created from SiNC amorphous powder. SiNC precursor decomposed to SiC and Si3N4 particles during sintering. The comparison of nano- and macro-hardness of investigated ceramic materials showed that nano-hardness is significantly higher. The indentation modulus correlated with the measured nano-hardness. Remarkable influence of grain boundaries and SiC nano-inclusions on hardness was observed.

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