Kumada Rearrangement of Polydimethylsilane Using a Catalytic Process |
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| Journal | Key Engineering Materials (Volumes 317 - 318) |
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| Volume | The Science of Engineering Ceramics III |
| Edited by | T. Ohji, T. Sekino and K. Niihara |
| Pages | 85-88 |
| DOI | 10.4028/www.scientific.net/KEM.317-318.85 |
| Citation | Young Hee Kim et al., 2006, Key Engineering Materials, 317-318, 85 |
| Online since | August, 2006 |
| Authors | Young Hee Kim, Dong Geun Shin, Hyung Rae Kim, Doug Young Han, Young Un Kang, Doh Hyung Riu |
| Keywords | Catalytic Process, Kumadar Rearrangement, Polycarbosilane, Polydimethylsilane |
| Abstract | Polycarbosilane was synthesized from polydimethylsilane in the presence of ZSM-5 (Si/Al=30) as a catalyst at 350oC-400oC. Characterization of synthesized polycarbosilane was performed with 29Si Solid NMR, FT-IR, and GPC analysis. Number average of molecular weight (Mn) of the polycarbosilane was ranged from 350 to 2340. |
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