Paper Title:
Preparation and Characterization of Kaolinite-Glucose Intercalation Compound
  Abstract

Kaolinite-glucose intercalation compound was synthesized by the intercalation of polar organic big molecule dodecylamine and then displaced by glucose in the layer of kaolinite. XRD, FT-IR, TG and DSC were used to study the reaction process and the characters of the products. The results indicated that the basal spacing of kaolinite increased to 2.280 nm from 0.717 nm, and the hydrogen bonds were formed between dodecylamine NH and kaolinite Si-O after dodecylamine intercalation. Kaolinite-dodecylamine intercalation compound was stable below 295 °C. After displacement reaction by glucose, the basal spacing of kaolinite increased to 3.364 nm, and the intercalation rate reached 87%, the hydrogen bonds were formed between glucose C=O and kaolinite inner surface hydroxyl. Kaolinite-glucose intercalation compound was stable below 302 °C.

  Info
Periodical
Key Engineering Materials (Volumes 368-372)
Edited by
Wei Pan and Jianghong Gong
Pages
1068-1070
DOI
10.4028/www.scientific.net/KEM.368-372.1068
Citation
L. Gao, L. J. Wang, Y. T. Du, G. W. Zhang, "Preparation and Characterization of Kaolinite-Glucose Intercalation Compound", Key Engineering Materials, Vols. 368-372, pp. 1068-1070, 2008
Online since
February 2008
Export
Price
$32.00
Share

In order to see related information, you need to Login.

In order to see related information, you need to Login.

Authors: Jian Yang, Tai Qiu, Chun Ying Shen
Abstract:An organic precursor was synthesized with C3N6H6 and H3BO3 as raw materials in aqueous solution. A novel amorphous BCN compound was obtained...
1080
Authors: Lin Jiang Wang, Da Qing Wu, Xiang Li Xie, Wen Feng Zhu, Li Gao
Abstract:The kaolinite-polyacrylamide intercalation compound was prepared by the displacement reaction of the kaolinite-formamide intercalation...
1093
Authors: Zhi Feng Lin, Shu Fang Zhang, Dun Zhang
Abstract:A supramolecular compound, Co(C5H4NCOO)2(H2O)2∙2H2O was hydrothermally synthesized and characterized by elemental analysis, infrared spectra,...
1475
Authors: Yan Xia Song, Chong Chen Wang, Yuan Lan Wang
Abstract:Two two-dimensional and three-dimensional coordination-polymer, [Ni(2,2′,5,5′-bpdc) (H2O)]•H2O (1) and[Ni(2,2′,6,6′-bpdc)2]•4H2O (2) were...
144
Authors: Zeng Hai Zhang, Guang Ming Wu, Guo Hua Gao, Wei Feng, Xiao Bo Jin, Jun Shen
Abstract:Sol-gel tequnique was used to prepare disordered tungsten oxide and molybdenum oxide sols. A series ratio of W:Mo compound sols were obtained...
184