Paper Title:
Synthesis, Properties and Characterisation of Manganeous Layered Double Hydroxides Using In Situ X-Ray Techniques
  Abstract

Synthetic manganeous Layered Double Hydroxides of the Hydrotalcite- and Shigaite- type were prepared by the coprecipitation method. The thermal behaviour of two compounds, [Mn6Al3(OH)18] [(SO4)2Na·12H2O] and [Mn6Al3(OH)18] [Cl·4H2O] was investigated by several experimental techniques. Thermal analysis and in-situ X-ray diffractometry show several dehydration stages of the synthesis products in the temperature range of 25 < T < 170°C followed by decomposition at temperatures above 200°C.

  Info
Periodical
Materials Science Forum (Volumes 443-444)
Edited by
Yvonne Andersson, Eric J. Mittemeijer and Udo Welzel
Pages
307-310
DOI
10.4028/www.scientific.net/MSF.443-444.307
Citation
U. König, H. Pöllmann, "Synthesis, Properties and Characterisation of Manganeous Layered Double Hydroxides Using In Situ X-Ray Techniques", Materials Science Forum, Vols. 443-444, pp. 307-310, 2004
Online since
January 2004
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Price
$32.00
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