Paper Title:

Unidirectional Solidification of a Nbss/Nb5Si3 In-Situ Composite

Periodical Materials Science Forum (Volumes 475 - 479)
Main Theme PRICM-5
Edited by Z.Y. Zhong, H. Saka, T.H. Kim, E.A. Holm, Y.F. Han and X.S. Xie
Pages 745-748
DOI 10.4028/www.scientific.net/MSF.475-479.745
Citation X.P. Guo et al., 2005, Materials Science Forum, 475-479, 745
Online since January, 2005
Authors X.P. Guo, Ping Guan, X. Ding, Jun Zhang, K. Kusabiraki, Heng Zhi Fu
Keywords Eutectic In Situ Composite, Microstructural Evolution, Niobium Silicide, Ultrahigh Temperature Alloy, Unidirectional Solidification
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Abstract

The directionally solidified specimens of Nb-13.52 Si-22.60 Ti–6.88 Hf–2.54 Cr–2.24 Al alloy were prepared in an electron beam floating zone melting furnace at the withdrawing rate of 0.1, 0.3, 0.6, 1.0, 2.4 and 6.0 mm/min. All the primary Nb solid solution (Nbss) columns, Nbss + (Nb)3Si/(Nb)5Si3 eutectic colonies and divorced (Nb)3Si/(Nb)5Si3 plates or chains align well along the longitudinal axis of the specimens. With increasing of the withdrawing rate, the microstructure is gradually refined, and the amount of Nbss + (Nb)3Si/(Nb)5Si3 eutectic colonies increases. Both the room temperature ultimate tensile strength σb and fracture toughness KQ are improved for the directionally solidified specimens. The tensile fracture occurs in a cleavage way.