Paper Title:
Mechanochemical Synthesis of Bi4Ti3O12
  Abstract

Our efforts were directed to the preparation of bismuth titanate – Bi4Ti3O12 (BIT) by mechanically assisted synthesis. The mechanical activation was applied to prepare bismuth titanate, Bi4Ti3O12, from bismuth oxide, Bi2O3, and titanium oxide, TiO2 (in an anatase crystal form). Mechanochemical synthesis was performed in a planetary ball mill in air atmosphere. Bismuth titanate ceramics was obtained by sintering at 1000 oC. The formation of Bi4Ti3O12 in the sintered samples was confirmed by X-ray diffraction analysis. Scanning electron microscopy, SEM, was used to study the particle size and powder morphology. The obtained results indicate that Bi4Ti3O12 from the powder synthesized by high-energy ball milling exhibits good sinterability, showing advantage of the mechanochemical process over conventional solid-state reaction.

  Info
Periodical
Edited by
Dragan P. Uskokovic, Slobodan K. Milonjic and Dejan I. Rakovic
Pages
125-130
DOI
10.4028/www.scientific.net/MSF.518.125
Citation
Z.Ž. Lazarević, B.D. Stojanović, J. A. Varela, "Mechanochemical Synthesis of Bi4Ti3O12", Materials Science Forum, Vol. 518, pp. 125-130, 2006
Online since
July 2006
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$32.00
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