Paper Title:

Preparation of Porous Glass Scaffolds by Salt Sintering Technique

Periodical Materials Science Forum (Volumes 587 - 588)
Main Theme Advanced Materials Forum IV
Edited by António Torres Marques, António Fernando Silva, António Paulo Monteiro Baptista, Carlos Sá, Fernando Jorge Lino Alves, Luís Filipe Malheiros and Manuel Vieira
Pages 52-56
DOI 10.4028/www.scientific.net/MSF.587-588.52
Citation Erika Davim et al., 2008, Materials Science Forum, 587-588, 52
Online since June, 2008
Authors Erika Davim, Maria Helena F.V. Fernandes, Ana Maria R. Senos
Keywords Calcium Phosphate Glass, Porous Scaffold, Salt Leaching
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Abstract

This paper reports a preliminary study on the development and characterization of a porous calcium phosphate glass-ceramic for tissue engineering application. To obtain porous glass scaffolds, a mixture of 3CaO.P2O5-SiO2-MgO glass (grain size below 20 'm) and NaCl with 200- 300 'm of particle size was taken in the volume proportion 1:1. The mixture was shaped into cylindrical samples (10 mm diameter x 10 mm thick) by using unidirectional pressing. The sintering thermal cycle was selected by means of thermal analyses (DTA/TG and dilatometry) in order to attain a high enough cohesion among the glass particles. After thermal consolidation, the salt was dissolved in water, resulting in highly porous materials. The effect of the sintering thermal cycle on the structure and microstructure characteristics of the scaffolds was investigated in this paper.