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Growth of 4H-SiC Single Crystals on 6H-SiC Seeds with an Open Backside by PVT Method

Journal Materials Science Forum (Volumes 615 - 617)
Volume Silicon Carbide and Related Materials 2008
Edited by Amador Pérez-Tomás, Philippe Godignon, Miquel Vellvehí and Pierre Brosselard
Pages 15-18
DOI 10.4028/www.scientific.net/MSF.615-617.15
Online since March, 2009
Authors Emil Tymicki, Krzysztof Grasza, Katarzyna Racka-Dzietko, Marcin Raczkiewicz, Tadeusz Łukasiewicz, Maciej Gała, Kinga Kościewicz, Ryszard Diduszko, Rafał Bożek
Keywords 4H-SiC, 6H-SiC Seed, Crystal Growth, Hexagonal Voids, Open Backside, PVT
Abstract 4H-SiC single crystals grown by the seeded physical vapour transport method have been investigated. These crystals were grown on 6H-SiC seeds. The influence of the seed temperature, form and granulation of SiC source materials on the stability and efficiency of the 4H polytype growth have been investigated. A new way of the seed mounting - with an open backside - has been used. Crystals obtained were free of structural defects in the form of hexagonal voids. The crystalline structure of SiC crystals was investigated by EBSD (Electron Backscatter Diffraction) and X-Ray diffraction methods. Moreover, defects in crystals and wafers cut from these crystals were examined by optical, scanning electron and atomic force microscopy combined with KOH etching.
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