Paper Title:

Surface Nanocrystallization of Zircaloy-4 by Surface Mechanical Attrition Treatment

Periodical Materials Science Forum (Volume 658)
Main Theme Eco-Materials Processing and Design XI
Edited by Hyungsun Kim, JianFeng Yang, Tohru Sekino, Masakazu Anpo and Soo Wohn Lee
Pages 452-455
DOI 10.4028/www.scientific.net/MSF.658.452
Citation Cong Hui Zhang et al., 2010, Materials Science Forum, 658, 452
Online since July, 2010
Authors Cong Hui Zhang, Xiao Ge Duan, Lian Zhou, Xin Zhe Lan
Keywords Dislocation, Nanocrystallisation, SMAT, Twin, Zircaloy 4
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Abstract

A nanostructured surface layer was induced on zircaloy-4 by the method of surface mechanical attrition treatment (SMAT). X-ray diffraction and microhardness tester were applied to identify the average grain size and hardness of specimen processed for different duration, transmission electron microscopy and high-resolution transmission electron microscopy were adopted to observe the microstructure of specimen. The results showed that the surface hardness enhanced gradually and then stabilized with the processing duration increasing, while the average grain size declined gradually, to the minimum 20 nm at 15 min, then increased. The formation of nanocrystalline was due to the mechanical twins and dislocation slip.