Paper Title:
One Step Solvothermal Synthesis of Flower-Like β-In2S3 Microstructures
  Abstract

Uniform 3D flower-like β-In2S3 microstructures were synthesized using InCl3·4H2O and KSCN as starting reagents in ethylene glycol at 200-220°C for 30h under solvothermal conditions. The prepared products were characterized by various techniques, such as XRD, XPS, FESEM, TEM and ED. FESEM and TEM observation reveals that the as-prepared flower-like β-In2S3 microstructures are assembled by plate-like nanocrystals with average thickness of 10nm. These nanoplates interconnect with each other to form an entangled network-like architecture with irregular-shaped pore in the flower-like β-In2S3 microstructures. Photoluminescence (PL) spectrum indicates that the synthesized β-In2S3 porous micro spheres have shown considerably greater quantum size effects.

  Info
Periodical
Materials Science Forum (Volumes 663-665)
Edited by
Yuan Ming Huang
Pages
982-985
DOI
10.4028/www.scientific.net/MSF.663-665.982
Citation
C. H. Deng, H. M. Hu, G. Q. Shao, "One Step Solvothermal Synthesis of Flower-Like β-In2S3 Microstructures", Materials Science Forum, Vols. 663-665, pp. 982-985, 2011
Online since
November 2010
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Price
$32.00
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