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A Study on the Preparation of Nano-Crystalline Barium Titanate Powder by a Sol-Gel Method

Journal Solid State Phenomena (Volumes 121 - 123)
Volume Nanoscience and Technology
Edited by Chunli BAI, Sishen XIE, Xing ZHU
Pages 53-56
DOI 10.4028/www.scientific.net/SSP.121-123.53
Citation J. Azadmanjiri et al., 2007, Solid State Phenomena, 121-123, 53
Online since March, 2007
Authors J. Azadmanjiri, Hojjatollah K. Salehani, A. Dehghan Hamedan, M. Sadeghi
Keywords Barium Titanate, Nano, Powder, Sol-Gel
Abstract

In this work, high purity BaTiO3 (BT) nano-powders by a sol-gel process was prepared with Ba(NO3)2 and Ti(C4H9O)4 materials in order to acquire uniform size grains. The effects of the crystallinity, microstructure of BT nano-powders calcined at different temperatures and dielectric properties of the ceramics were investigated by XRD, SEM and impedance analyzer, respectively. Scanning electron microscopy and X-ray diffraction investigation revealed cubic plates and crystallite size. The results revealed that crystallite size and calcination temperature of BT and influence on the dielectric constant.

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