X-Ray Diffraction and Electric Measurements of Phase Transformation in Li-Mn Spinels |
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| Journal | Solid State Phenomena (Volume 130) |
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| Volume | APPLIED CRYSTALLOGRAPHY XX |
| Edited by | Danuta Stróż & Małgorzata Karolus |
| Pages | 63-68 |
| DOI | 10.4028/www.scientific.net/SSP.130.63 |
| Citation | J. Pielaszek et al., 2007, Solid State Phenomena, 130, 63 |
| Online since | December, 2007 |
| Authors | J. Pielaszek, J.R. Dygas, F. Krok, D. Lisovytskiy, Monika Kopeć, M. Marzantowicz |
| Keywords | Electric Measurements, Lithium-Manganese Spinels, Phase Transformation, X-Ray Diffraction (XRD) |
| Abstract | Laboratory prepared and commercial Li-Mn spinels were studied. Making use of the dedicated XRD-impedance spectroscopy experimental set-up, direct correlations of the degree of phase transformation (expressed as change of the FWHM of the selected reflection) with electric conductivity was found. Independent XRD measurements and full pattern fitting allowed quantitative estimations of the phase composition of the spinels. It was found that commercial spinels were in fact multiphase, with the content of the additional phase of few weight percent. |
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