Papers by Author: B.J. Choi

Abstract: he aim of this study was to evaluate the effect of HA on the demineralization resistance and bonding strength of light-curing glass ionomer dental cement. Tests were conducted using (1) pure Fuji II LC GIC, (2) 15% micro HA-Fuji II LC GIC. Physical properties, demineralization resistance and bonding strength to dentin of teeth were determined. The curing depth in all groups were satisfied the requirement of curing depth of ISO 9917-2:2004(minimum curing depth = 1mm). The depth of cure was reduced with addition of HA, presumably due to the light scattering effect of HA particles. Regarding sensitivity to ambient light, there were no detectable changes of the homogeneity in any groups. Also all groups were satisfied the requirement of the flexural strength of ISO 9917-2:2004(minimum flexural strength = 20MPa). 15% HA-Fuji II LC GIC group was found to present a greater flexural strength than pure Fuji II LC GIC, as the addition of HA promotes a chemical reaction between the HA, the glass powder, and the polyacid. Observing under the CLSM after 4 days of demineralization, there were significant differences in the CLSM and SEM images. Pure Fuji II LC GIC group showed greater enamel demineralization layer than in 15% HA-Fuji II LC GIC group. In SEM analysis, there was greater enamel demineralization in the pure Fuji II LC GIC group, and less demineralized under the influence of HA particles, 15% HA-Fuji II LC GIC group had more even surface particles. 15% HA-Fuji II LC GIC group was found to present a greater bonding strength than pure Fuji II LC GIC group. Observing the fractured surfaces under SEM after the bonding strength test, the cohesive failure rate was found to be in increasing order of pure Fuji II LC GIC, 15% HA-Fuji II LC GIC group. There were bone-like apatite particles observed to be formed in 15% HA-Fuji II LC GIC group.

Abstract: This study aimed to evaluate the anticariogenic and remineralization effects of the glass ionomer dental luting cement containing nano-β-TCP in vitro. The β-Tricalcium Phosphate (β-TCP) are the components of dental enamel and bone mineral as biological apatites. In addition, β-TCP contains a significant amount of calcium and phosphate, which can promote remineralization of enamel subsurface lesions in animal and human. RelyXTM glass ionomer cement(3M/ESPE, USA) was used as dental luting cement. Film thickness, setting time, and compressive strength was measured for each group of pure glass GIC, 15% nano-β-TCP GIC. Human molars were prepared in box-shaped cavities that were filled with the GIC with and without the 15% nano-β-TCP were placed in 25ml of pH 5.0 acid buffer for 4 days at 37°C. After 4 days, longitudinal sections (1007m) were obtained through the center of each restoration. The sections were analyzed using a scanning electronic microscope (SEM) and confocal laser scanning microscopy (CLSM) to identify the change in the enamel surface. A significant difference in the CLSM images between pure GIC and nano-β-TCP-GIC. CLSM allows the demineralized surface layers of sound enamel to be visualized down to approximately 100 μm. The pure GIC specimens had a relatively thick fluorescent layer. On the other hand, the fluorescent layer of the nano-β-TCP-GIC specimens were thinner. The SEM images of micro surfaces demonstrate that nano-β-TCP-GIC is less rough than pure GIC. Therefore, the addition of nano-β-TCP enhanced protection against acid demineralization and promoted remineralization of enamel surface.

Abstract: Histoacryl® (N-butyl-2-cyanoacrylate) has been widely utilized as a tissue adhesive. The aim of this study was to evaluate the physical and adhesive properties of newly developed cyanoacrylate-based β-TCP composite systems. The β-TCP powder was modified on the surface with citric acid to make this material mixed with cyanoacrylate easily. The setting time of acidtreated β-TCP/ Histoacryl® systems was dramatically prolonged and the polymerization heat was significantly decreased compared to that of untreated β-TCP/Histoacryl® system. The shear bond strength of cyanoacrylate-based β-TCP composites decreased with addition of acid-treated β-TCP filler. The compressive strength of β-TCP/Histoacryl® composites increased strongly with increasing the amount of acid-treated β-TCP filler. The cytotoxicity of the β-TCP/Histoacryl® composites decreased with the increasing of the amount of added β-TCP. These results indicated that our novel β-TCP/Histoacryl® composites had the great potential to serve as adhesives or filling materials in the dental field.

Abstract: The mineral phase of bone and teeth is mainly hydroxyapatite. Currently there are numerous researches being conducted on the effect of the addition of hydroxyapatite to dental materials. Among them, several studied were published stating that the addition of hydroxyapatite to composite resin or glass ionomer cement resulted in an improvement in bonding strength and physical properties Therefore, this study will investigate the effect that the addition of hydroxyapatite to light curing glass ionomer cement has on bonding strength. Two different light curing glass ionomer cement products were selected (FujiⅡLC, GC Cor, Japan and Vitremer™ , 3M/ESPE, USA) and hydroxyapatite was mixed into the light curing glass ionomer cement at various concentrations to create hydroxyapatite-light curing glass ionomer cement mixture. In order to confirm that hydroxyapatite-light curing glass ionomer cement met the basic requirements of dental materials, sensitivity to ambient light, depth of cure, and flexural strength were tested. From the results of the above mentioned tests, the hydroxyapatite-light curing glass ionomer cement with the most superior physical properties for each product (15% HA-Fuji Ⅱ LC, 20% HA-Vitremer™)was bonded to the teeth and then immersed in artificial saliva(36.5°C) for four weeks. Finally the sectioned surface was observed under SEM after measuring the bonding strength. As the hydroxyapatite concentration increased, the depth of cure decreased. However flexural strength increased and there was not much change in the sensitivity to ambient light. Bonding strength, which was the main focus of this study, increased with the addition of hydroxyapatie and scanning electron microscope findings show a more cohesive type of fracture in the material with bone like apatite material formation along the tooth-material interface.

Abstract: The purpose of this study is to investigate the remineralization of enamel in the human tooth by fissure sealant containing various amount of hydroxyapatite. Prior to remineralization experiments, the necessary requirements of the dental fissure sealant, the curing depth and the curing time, were measured with the content of the hydroxyapatite according to the standard of ISO 6874. Various amount of hydroxyapatite was mixed uniformly using sonicator up to 20 wt% to the fissure sealant. In spite both the curing time and the curing depth were decreased with increasing the content of hydroxyapatite, all samples were satisfied the ISO requirements. Remineralization experimental samples were produced by bonding fissure sealant containing various amount of hydroxyapatite to human tooth enamel using manufacturer’s information. After exposure to the simulated body fluid at 36.5oC for 4 weeks, the bonding strength and the surface morphology were examined using Instron and scanning electronic microscope, respectively. The bonding strength between the fissure sealant and the human teeth was drastically enhanced with the amount of hydroxyapatite. The remineralization zone could be observed along with the boundary of hydroxyapatite and fissure sealant using a scanning electronic microscope.