Papers by Author: Chang Chun Ge

Abstract: Sintered and forged powder metallurgy (P/M) steels were subjected to tensile, hardness and impact test, in order to understand the influence of the microstructure on the mechanical properties and fracture behavior. Ultimate tensile strength, yield strength, elongation, reduction in area, hardness and impact toughness all increase with a decrease in porosity. With the increase of density, the mode of fracture change from pure ductile in sintered necks of the material to complete brittle from fully dense pearlitic grains.

Abstract: Nuclear fusion is a promising source of environmental friendly energy for the future, and the ultra-fine grained Tungsten (W) is a hopeful candidate material to be used as plasma-facing materials (PFMs), which are the key materials in the International Thermonuclear Experimental Reactor (ITER), for its many useful advantages. While, due to its high melting point and high sintering temperature needed, the ultra-fine grain sized tungsten is not easy to be fabricated. In this paper, the method of explosive consolidation of powders as well as its mechanism and improvements are discussed, and finally the possibility of using this method to preparing of ultra-fine grained W plasma facing material are also introduced.

Abstract: In this article we present the testing, evaluation of infrared radiation properties of polycrystalline materials especially as cordierite-based glass-ceramics. Researches aim to make a comprehensive and systematic exposition of emissivity definition, test principles and test methods. And on the basis of measurement results of the infrared emissivity of cordierite-based glass-ceramics, the Infrared radiation property of this polycrystalline material was discussed. Research has a positive significance on the development of the infrared radiation heating and drying materials.

Abstract: In this article we present a new kind of large grain transparent glass-ceramics obtained by the method of crystal growth from a homogenous glass, the simultaneous variation of the glass matrix and crystalline compositions during the crystallization results in the high transparency of this kind of large grain, high crystalline volume glass-ceramics, which have suitable refractive indexes between respective phases. The nucleation and crystallization behaviors of this kind of glass-ceramics have been investigated. The optimum heat treatment schedule for the glass was determined by means of DSC, XRD and SEM. The desirable optical property, such as laser characteristics etc, of this new kind of glass-ceramics can be further developed by doping with transition metals or rare-earths.

Abstract: Two kinds of W/Cu functionally graded material based high heat flux components, including monoblock concept and flat tile concept, are designed and fabricated. Thermally induced stresses and strains under operation conditions in these components are analyzed using finite element analysis. The effect on stress and strain of using different graded structures to join Cu to W is examined and compared. There has no obvious difference on operation thermal stress mitigating between monoblock design and flat tile design. The component with monoblock concept was fabricated by a one step fast resistance sintering, and the component with flat tile concept was fabricated by infiltration-welding method successfully.

Abstract: Tungsten has been decided as the plasma facing material (PFM) for some high heat flux regions of the divertor in the International Thermo-Nuclear Experimental Reactors (ITER). In this paper, our efforts concentrated on the functionally gradient W/Cu coating fabricated on the oxygen free copper by atmosphere plasma spraying under the inert gases protection. The functionally gradient W/Cu coatings were designed to relieve the thermal stress during the spraying processes. For comparison, the tungsten coatings were also deposited directly onto the copper substrates by the same technology. XRD, SEM and EDS were applied to identify the phases, morphologies and compositions of these coatings. Tensile tests were performed to measure the bonding strength between the coatings and the substrates. Furthermore, water quenching and high heat loading experiments using a pulse laser beam were also carried out to estimate the thermal shock properties of these coatings.

Abstract: The B4C/BN laminated ceramics were prepared by tape casting/coating. The effect of structure on the mechanical behavior of the B4C/BN was studied. The results showed that the fracture toughness and bending strength are optimal when the layer thickness ratio (eB4C/eBN) is 15. The SEM photographs of B4C/BN laminated ceramic indicated that the high fracture energy mainly resulting from crack deflection and crack delamination at the BN weak interface.

Abstract: This paper reports some new progresses on layered and graded coatings for plasma facing materials in fusion devices in Laboratory of Special Ceramics and Powder Metallurgy (LSCPM), University of Science and Technology Beijing (USTB), China. They included tungsten coatings made be various particle sizes of initial feedstock and interlayers and boron carbide graded coatings. All the coatings were fabricated on the oxygen free copper by plasma spraying. The microstructures and properties were investigated for PFM. Water quenching and high heat loading experiments were also carried out to estimate the thermal performance of these coatings.

Abstract: Several kinds of ceramic powders including SiC, TiO2 and Al2O3 were selected as fillers blending with epoxy resin, curing agent and other additives to prepare a heavy-duty and anti-wear coating. The effects of filler sort, powder size, dispersion homogeneity on the coating properties were investigated. The results showed that the wear resistance and corrosion resistance of the coating could be improved significantly after meliorating the dispersion of the ceramic particles in epoxy resin. Other mechanical properties were also studied in order to support the view on the positive effect of the nano-particles in the epoxy coating.

Abstract: Selective laser sintering (SLS) of Si3N4 and Al2O3 powders were investigated in this work. Copolymer was synthesized through monomer MMA and BMA. Infrared spectrum was employed to characterize the as-synthesized copolymer. Results show that the main compositions of the copolymer are PMMA and PBMA. The binders were prepared by mixing the copolymer and the inorganic NH4H2PO4 with certain ratio. Binders were used to coat the Si3N4 and Al2O3 powders by spray drying. The coated powders were sintered successfully by SLS to make cubic part and rotor part.