Papers by Author: Dong Hyuk Shin

Abstract: In this study, dynamic deformation behavior of submicrocrystalline aluminum alloy was established with respect to equal-channel angular (ECA) pressing routes such as A, B, and C. After 8-pass ECA pressings, the deformed samples, regardless of the routes applied, were consisted of ultrafine grains together with high dislocation density near the boundaries. Microstructural observation revealed that the sample deformed via route B showed more diffused diffraction pattern than those deformed via route A and C, suggesting the fact that route B was most effective for a rapid evolution in the grain boundary orientation from low-angle to high-angle characteristics. In the torsion tests, the shear stress decreased once reaching the maximum point. This maximum was the highest in the sample deformed via route B, and decreased in the order of the route C and route A. The dynamic deformation was explained based on microstructural uniformity associated with ECA pressing routes.

Abstract: Characterization of nickel oxide layers on the AZ91 Mg alloys by plasma electrolytic oxidation (PEO) was investigated. For this purpose, PEO coating was carried out on the present sample in the alkaline electrolyte with nickel ion at three different voltage responses, i.e., 150, 250, 350 V. The amount of nickel oxide increased by increasing process time, and changed the color of sample from light grey to moderate olive brown. It was observed from potentio-dynamic polarization analysis that polarization resistance of oxide layer was increased with increasing nickel ions. Also microhardness of the sample processed at 350 V was higher than those of the samples.

Abstract: An attempt has been made to clad Mg alloy with Al by twin-roll casting. This was done by inserting an Al sheet between the roll and the Mg alloy melt during twin-roll casting. Microstructural investigation across the transverse section of the as-cast Al-clad Mg alloy sheet reveals a very good interfacial bonding between Al and the base Mg alloy. Annealing of the Al-clad Mg alloy sheet results in the formation of layers of various intermetallic phases along the Mg/Al interface. Subsequent rolling of the as-annealed sheet significantly improves the formability of the reaction zone, as evidenced by the cracking of the base Mg alloy before the cracking of the reaction zone.

Abstract: The low cycle fatigue(LCF) test was performed to characterize the influences of the equal channel angular pressing(ECAP) and subsequent annealing of Al 5052 alloy. In the present research, one group of Al 5052 alloy specimens was directly subjected to ECAP, while another was subjected to ECAP and subsequent annealing. It was found that the tensile strength of the Al 5052 alloy increased, while its elongation decreased, with increasing number of ECAP passes. The LCF test was conducted at constant total strain amplitudes of 0.5%, 0.7%, 0.9% and 1.1%. Only cyclic hardening was observed as the number of fatigue cycles increased at all strain amplitudes in the specimen without ECAP. However, the ECAPed specimens showed a slight amount of cyclic hardening in the beginning and then saturation until fracture.

Abstract: The effects of equal channel angular pressing (ECAP) and subsequent heat treatment on the low cycle fatigue properties of 6005 Al alloy were investigated. The ECAPed specimens showed cyclic softening, whereas the peak aged specimens showed cyclic hardening at all strain amplitudes. After ECAP, artificial aging was performed at 175°C to observe the change of the low cycle fatigue properties due to precipitation. The fatigue life and behavior of the unECAPed and ECAPed 6005 Al alloys were discussed in terms of the microstructural changes and aging conditions.

Abstract: It is well known that the utilization of superplastic characteristics in manufacturing process makes many of aerospace components lighter and stiffer. The weight saving is vitally important especially for aerospace application and even more weight saving is possible when the superplastic forming is carried out with diffusion bonding. In this study, the lightweight sandwich structure was fabricated with superplastic forming(SPF) process from diffusion bonded(DB) Ti-6Al-4V sheets. The solid state diffusion bonding process was conducted in non-vacuum environment under a pressure of 4MPa for 60 minutes at 875°C and the superplastic forming process was followed for another 40 minutes. Good solid state bonding interface have been observed in microstructure observation and the sandwich structure was successfully manufactured. It is important to note that the forming conditions of present study are more practical for application than the previously published conditions, which require vacuum environment, higher temperature and/or pressure.

Abstract: Ultrafine grained (UFG) 5083 Al and 5154 Al alloys were prepared by equal channel angular pressing (ECAP) with an effective strain of ~ 4 or ~ 8. This investigation was aimed at examining the effect of the ECAP strain and post-rolling inducing different microstructure in these alloys on the deformation mechanisms at low temperature superplastic (LTS) and high strain superplastic (HSRS) regimes. The sample after 4 passes (a strain of ∼ 4) did not exhibit LTS, but superplastic elongations were obtained in the sample after 8 passes (a strain of ∼ 8). An analysis of the mechanical data in light of the standard deformation mechanisms revealed that deformation of the sample after 4 passes was governed by dislocation climb while grain boundary sliding attributed to LTS of the sample after 8 passes. In addition, the 5154 Al alloy processed by ECAP and postrolling was capable of enhancing HSRS elongation significantly. An analysis revealed that the deformation mode was changed from dislocation viscous glide to grain boundary sliding by additional ECAP strain and post-rolling.

Abstract: It is known that Ti-6Al-4V alloy is one of the excellent candidates for aerospace structure due to their high specific strength.However, its higher cost and low formability relative to other materials tend to limit the wide usage of the material.The purpose of this study is to characterize the superplasticity of this alloy so to obtain materials and process parameters for superplastic forming and diffusion bonding for industrial application. High temperature tensile tests was carried out at the strain rate range of 10-4 to 10-2 s-1 and temperature range of 1123°C to 1223°C. According to the results of the experiment, the optimum diffusion bonding condition was obtained at 1148°C, applying pressure of 4MPa for 1 hour in argon gas environment, which condition is more practical than expensive vacuum condition. It is shown that at the optimum condition for diffusion bonding with parent metal, the oxide film becomes unstable and the oxygen is diffused into the bulk. At this condition, the mechanical and microstructural integrity at the bonding interface was observed in a sandwich structure and a heavy block of titanium part from massive diffusion bonding process.

Abstract: To study the effect of grain size on texture and tensile properties of equal channel angular pressed commercially pure Ti, specimens were made to have the grain size ranging from 4 m to 60 m with the severe plastic deformation followed by recrystallization annealing. In this initial condition all the specimens exhibited a strong bimodal split basal texture. During subsequent repressing at 350°C, the texture pattern became randomized through crystal rotations, the phenomenon being more pronounced in coarse-grained specimens. The microstructure of deformed specimens, as examined by electron back scattered diffraction, showed formation of mechanical twins and microstructural inhomogeneity in the coarse-grained specimens. The room temperature tensile properties of the re-pressed specimens showed that the yield strength was remarkably enhanced regardless of the grain size whereas the elongation was reduced as compared to the initial condition, particularly in coarse-grained specimen. It was concluded that microstructural refinement during the severe plastic deformation was the main cause of the improved yield strength while the twinning and microstructural inhomogeneity were responsible for the texture randomization and the impaired ductility.