Papers by Author: Enrique Díaz Barriga-Castro

Abstract: The aim of the present work is to determine the austenite to ferrite transformation temperatures in a Si-Al non-oriented electrical steel. Critical transformation temperatures on heating and cooling are determined using an in-situ X-ray diffraction technique where the specimen is heated or cooled in a stepwise manner. The transformation temperatures are estimated from changes in the intensities of the (110)α and (111)γ peaks as a function of temperature. The time evolution of the microstructure resulting from isothermal heat treatments at temperatures between 800 and 1000 °C applied after cooling from 1050 °C is followed by quantitative metallography on samples quenched into water. The results show that, on cooling, formation of ferrite starts at about 950 °C and ends at 790 °C, indicating a strong effect of Si and Al on the austenite to ferrite and eutectoid transformations. These results suggest that the low tensile ductility exhibited by this material at temperatures near 1000 °C can be attributed to strain localization in strain-induced ferrite formed at temperatures as high as 1025 °C.

Abstract: Wavelet analysis and bispectrum was applied to Acoustic Emission (AE) signals from scratch tests on corroded hot-dip galvanized samples in order to achieve the detection of corrosion products in pieces non reachable by visual inspection. AE signals were correlated with the fracture mechanisms occurring during scratch tests, while the contact force increased. Results were corroborated by Scanning Electron Microscopy (SEM), Energy Dispersive X-ray spectroscopy (EDX) and X-Ray Diffraction (XRD).