Papers by Author: Faina Muktepavela

Abstract: One of the directions of application of the perforated metal material is their use as cutting elements in the production of processing tools. In this case it is necessary to carry out hardening of cutting surfaces to increase their hardness. One of the methods of hardening metals could be laser treatment. Therefore, the present work is a study of the effect of Nd:YAG laser radiation on the microstructure and hardness of fragments formed from steel perforated tape. Different laser scan speeds (doses) were used in the experiments. The results have shown that the increase the microhardness of 30-40% after the laser treatment of steel perforated tape in the surface layer in a depth range up to 1 μm take place. The studies of microstructure of fragments formed from steel perforated tape have shown the reduction of the structure size and the presence of a thin oxide compounds, which is consistent with the results on nanoindentation. Hardening of the metal by laser radiation is carried out without surface melting which eliminates the change of macroroughness and the need for subsequent machining process.

Abstract: Mechanical properties, microstructure of the Sn–38wt. %Pb eutectic and the development of deformation - induced diffusion processes on interphase boundaries (IB) were investigated. Experiments were carried out both in deformed and annealed states of eutectic using micro- and nanoindentation, SEM, AFM and optical microscopy techniques. It was found that the deformation of the annealed alloy is localized at the Pb/Sn interphase boundaries and occurs by grain boundary sliding (GBS) accompanied by sintering micropore processes under the action of the capillary forces on the Pb/Sn IB. During severe plastic deformation of Sn-Pb eutectic phase transition in the Sn grain boundary occurs. This deformation-induced process takes place due to the wetting of tin with Pb. These diffusion accommodation processes (sintering and wetting) are facilitated by the low values of the Pb/Sn interphase energy (0.07 J/m2). Wetting is thermodynamically favourable because the condition γgb > 2 γib is satisfied and it is also kinetically allowed due to the relatively high homologous temperature (> 0.5•Tm). The obtained values of the nanohardness and elastic modulus evidence that the IBs in the Sn–Pb eutectic have to be considered as a separate quasi-phase with its own properties.

Abstract: Properties of interfaces in solid state metal/oxide joints (Al/SiO2, Al/MgO, Al/glass, Mg/MgO, Mg/SiO2, In/glass etc.) are reported. The interfaces were formed by plastic deformation of metal on the oxide surface at room temperature. Their structure, chemical composition, and micromechanical properties were studied by the AFM, XRD, SIMS, optical microscopy, and precision microindentation techniques. A noticeable adhesion was observed for metals with high affinity for oxygen and only in the regions of the maximum shear stress. Formation of an interfacial reaction zone with an oxygen concentration gradient is detected. In this zone metals are nanostructured and noticeably hardened. The effect of mechanoactivation is considered as a result of physical and chemical interaction and formation of nanostructures in deformed metal/oxide systems.

Abstract: Mechanical properties of interphase boundaries (IB), stability of defects and microstructure in heavily deformed binary eutectics (Al-Sn, Zn-Sn, Pb-Sn, Cd-Sn, Bi-Sn) have been investigated at room temperature. Experiments were carried out on atomically clean surfaces of alloys and on bimetallic joints with clean interface. It has been shown that after severe deformation the phases are strengthened and relaxation processes occur mainly on the boundaries in all eutectics. For superplastic eutectics with low interphase boundary energy the intensive development of the diffusion – controlled processes of self- healing, sintering, segregation and enveloping were observed. These diffusion processes, directed to restoration of a contact, are the reason of softening of interphase boundaries and superplastic viscous flow. It has been shown that for the eutectics with high IB energy (Al−Sn, Zn−Sn) the interphase boundary sliding leads to the formation of narrow IB cracks with sharp angles. Diffusion healing of micropores and cracks on these IB does not develop at room temperature and deformation defects are stable. Such deformed structure of IB defines low temperature brittleness of Zn-Sn, Al-Sn eutectics and hydrogen brittleness of Al-Sn.