Authors: Makiko Hashiguchi, Hideo Sato, Y. Nishi, Seiji Ban, Kristoffer Krnel, Andraž Kocjan, Tomaž Kosmač
Abstract: The aim of this study was to investigate the effect of surface treatments on bonding
strength of two kinds of zirconia to two kinds of dental cements. After thermal cycling, the shear
bonding strength of both zirconia with alumina coating increased in both cements. The shear
bonding strength of both zirconia with sandblasting decrease in Fuji plus after thermal cycling
(p<0.05). There was no significant difference between NANOZR and Y-TZP (p>0.05). The bonding
strengths of NANOZR with the alumina coating were higher than those with sandblasting after
thermal-cycling (p<0.05).
575
Authors: Hideo Sato, Naoko Kubota, Seiji Ban, Youichi Yamasaki
Abstract: The aim of this study was to determine the biaxial flexure strength of a commercially available dental pulp capping or cavity liner material, mineral trioxide aggregate (MTA). MTA and a conventional pulp capping material, calcium hydroxide, were used in this study. Each material was prepared into a disk-shaped specimen. Those specimens were stored in 100% humidity atmosphere at 23 or 37°C for 3 or 24 h. Six specimens in each condition were used for the biaxial flexure test using a piston-on-three-ball according to ISO-6872. Surface pH values were determined. The biaxial flexure strengths of MTA after setting in 24h were larger than those of Dycal (p <0.01). pH value of MTA was higher than that of Dycal. These results indicated that MTA was clinically usage material.
429
Authors: Hideo Sato, Seiji Ban, Masahiro Nawa, Y. Suehiro, H. Nakanishi
Abstract: The aim of this study was to investigate the effect of surface treatments on bonding
strength of two kinds of zirconia to three kinds of resin cements. After thermal cycling, the shear
bonding strength of both zirconia decreased in all the resin cements. The bonding strengths of two
resin cements in which primer contains silane dramatically decreased after the thermal-cycling
(p<0.01). Although the surface roughness of both zirconia sandblasted by 125-%m SiC was quite
larger than that by 70-%m alumina (p<0.05), there were no significant differences in the bonding
strength of the resin cement to both zirconia sandblasted by 70-%m Al2O3 and 125-%m SiC
(p>0.05).
829
Authors: Daisuke Yamashita, Kenji Kanbara, Miho Machigashira, Motoharu Miyamoto, Hideo Sato, Yuichi Izumi, Seiji Ban
Abstract: The aim of this study was to evaluate the biocompatibility with the proliferation of
osteoblast-like cell (MC3T3-E1) on zirconia/alumina nanocomposite (NANOZR) in comparison to
yttria stabilized zirconia (3Y-TZP) and titanium (Ti). Cellular proliferations after 1-, 3-, 6-, and 9-day
incubation were calculated from the measurement of the MTT activities of the proliferated cell and
were analyzed by two-way ANOVA. Time-dependent proliferation of MC3T3-E1 in all the sample
was observed in all three materials with culture days. However, these were no significant differences
in the proliferation between three kinds of material, indicating all the materials have a similar-good
biocompatibility.
1099
Authors: Seiji Ban, Hideo Sato, Y. Suehiro, H. Nakanishi, Masahiro Nawa
Abstract: The effect of sintering condition, sandblasting and heat treatment on biaxial flexure
strengths of the zirconia/ alumina nanocomposite stabilized with cerium oxide (Ce-TZP/Al2O3
nanocomposite, referred to NANOZR) was evaluated in comparison to that of yttria stabilized
tetragonal zirconia polycrystals (Y-TZP). The disc-shaped specimens of NANOZR and Y-TZP
were cut from the full-sintered or middle-sintered ones. The discs cut from the middle-sintered
ones were finally sintered at the same temperature for the full-sintered one. These four kinds of
disc were treated in various conditions combined with the sandblasting, the heat treatment, and the
storage. The biaxial flexure strength of both middle- and full-sintered Y-TZP decreased with the
autoclaving, whereas those of both NANOZR did not change with it. The monoclinic content of
both the materials increased with the sandblasting and decreased with the heat treatment.
Regardless of the sintering condition, the monoclinic content of the Y-TZP dramatically increased
with the autoclaving and those of NANOZR remarkably increased with the sandblasting.
Regardless of the different surface roughness, the biaxial flexure strengths of both materials
strongly depended on the content of monoclinic ZrO2 on the surface.
779
Authors: Hideo Sato, Seiji Ban, Masahiro Nawa, Y. Suehiro, H. Nakanishi
Abstract: This study was aimed to investigate the effect of grinding, sandblasting by alumina and
SiC, and heat treatment on the phase transformation from tetragonal to monoclinic zirconia on the
surface of yttria stabilized tetragonal zirconia (Y-TZP) and zirconia/alumina nanocomposite
stabilized with cerium oxide (Ce-TZP/Al2O3 nanocomposite). The monoclinic phase content of both
materials increased with the grinding and the sandblasting, while it decreased with the heat
treatment. The monoclinic content sequentially increased with the sandblasting and decreased with
the heat treatment to each specific value. The SiC-sandblasting produced the larger monoclinic
content than alumina-sandblasting. Furthermore, the content changes of the nanocomposite were
larger than Y-TZP.
1263
Authors: Seiji Ban, Hideo Sato, Y. Suehiro, H. Nakanishi, Masahiro Nawa
Abstract: The effect of sandblasting and heat treatment on biaxial flexure strengths of the
zirconia/alumina nanocomposite stabilized with cerium oxide (Ce-TZP/Al2O3 nanocomposite) was
evaluated in comparison to that of yttria stabilized tetragonal zirconia polycrystals (Y-TZP). The
disc-shaped specimens of the nanocomposite and Y-TZP were sandblasted with 70)m alumina
powder. After sandblasting, half of the specimens were heated at 1000°C for 5 min. The biaxial
flexure strengths of Y-TZP were independent on the sandblasting, but decreased with the heat
treatment. On the other hand, the biaxial flexure strength of the nanocomposite increased with the
sandblasting and significantly decreased with the heat treatment. The content of monoclinic ZrO2 of
Y-TZP and the nanocomposite increased with the sandblasting pressure and dramatically decreased
with the heat treatment. These results suggest that the stress-induced transformation from tetragonal
to monoclinic of the nanocomposite occurs more easily than Y-TZP.
353
Authors: Hiroshi Kono, Motoharu Miyamoto, Hideo Sato, Seiji Ban
Abstract: An apatite coating by an alternate soaking was undertaken on commercially pure titanium (cpTi) treated with concentrated acid and alkaline solutions. X-ray diffraction (XRD) patterns indicated that the diffraction peak intensities assigned to hydroxyapatite (HAp) increased with the reaction cycle. Fourier transform infrared spectroscopic study (FTIR) showed similar results with
XRD. Scanning electron micrographs (SEM) of the deposits showed no observable change after the vacuum firing. It was confirmed that the reaction cycle greatly affected on the deposited amount of apatite on cpTi plates using the alternate soaking and the vacuum firing erased TiH2 formed during the acid etching, but was irrelevant to the crystallinity of the apatite.
679