Papers by Author: Irina P. Semenova

Abstract: The paper studies the microstructure of two-phase ultrafine-grained titanium VT8M-1 alloy (Ti-5.7Al-3.8Mo-1.2Zr-1.3Sn), which was obtained by rotary swaging (RS). Parameters of the microstructure and the change of the phase elemental / chemical composition were investigated by scanning electron microscopy and transmission electronic microscopy. It was shown that the silicide particles like S₂ - (Ti,Zr)₆Si₃ were precipitated in the process of rotary swaging_. The influence of silicide precipitations on the characteristics of high temperature strength of the ultrafine-grained two-phase titanium VT8M-1 alloy was discussed in the paper. The alloy microstructure was analyzed after the creep-rupture tests in the operation temperature range 300-400^oС.

Abstract: This paper is aimed to study the creep behavior of two-phase ultrafine-grained VT8M-1 (Ti-5.7Al-3.8Mo-1.2Zr-1.3Sn) titanium alloy obtained by rotary swaging (RS). It is shown that the 100-hour creep strength of the ultra-fine grained (UFG) VT8M-1 alloy retains high values at temperatures up to 400 °C. An increase in the testing temperature to >450 °C leads to a decrease in the creep rupture strength. The relationship between the microstructure and creep resistance of UFG alloy is discussed.

Abstract: This paper aims to study the peculiarities of a modified layer in the surface of ultrafine-grained (UFG) Ti-6Al-4V alloy after high energy ion nitrogen implantation. The UFG structure in the alloy was produced by equal channel angular pressing. X-ray diffraction analysis and scratch-testing were applied for the investigation. The influence of low-temperature annealing (400°C during 1 hour) on the substructure parameters and phase composition of the surface layer depending on a number of cycles of ion implantation with annealing was shown in the research. The effect of the UFG structure on mechanisms and strengthening degree of the surface after ion implantation is discussed.

Abstract: The paper focuses on the analysis of microstructure and mechanical properties of the Ti alloy VT8М-1 (Ti-5.3Al-4.0Mo-1.2Zr-1.3Sn-0.2Si) in an ultrafine-grained (UFG) state subjected to a long-term annealing at a service temperature of (≤ 450°С). A rotary swaging (RS) was used to process an UFG state in the material. The precipitation of disperse silicides of S2 was observed after the deformation by RS. It has been shown that the UFG alloy retained its high level of thermal stability and enhanced mechanical properties after long-term annealing up to 500 hours. The role of disperse silicides in both strengthening and stability of mechanical properties in the alloy after long-term annealing is discussed.

Abstract: The work addresses the microstructural evolution and mechanical properties of the ultrafine-grained (UFG) VT8M-1 subjected to isothermal die forging (IDF) and subsequent thermal treatment. An UFG microstructure with a mean size of secondary grains of about 0.3 μm was processed by a rotary swaging (RS) at Т=780°С. The ultimate tensile strength (UTS) of the alloy increased by 23% as compared to an initial state due to the formation of an UFG microstructure. It has been shown that isothermal die forging of the UFG alloy at Т=780°С leads to the growth of secondary phase grains by 0.7 μm. Subsequent heat treatment of the forged billets leads to hardening of 11%, which can be attributed both to the formation of additional interphase α/β boundaries at the precipitation of a tertiary α-phase and silicide dispersion.

Abstract: Recent studies have revealed that ultrafine-grained (UFG) metals and alloys produced by severe plastic deformation (SPD) can demonstrate extraordinary superplasticity at low temperatures and/or high strain rates. This work presents new results on superplasticity in several UFG Al and Ti alloys focusing on microstructural evolution and strain hardening, as well as the challenges of their application. Grain refinement in these alloys was accomplished using severe plastic deformation techniques, including new modifications of equal channel angular pressing (ECAP). Unusual behavior of UFG alloys originates both from the formation of ultrafine grain by SPD processing as well as the state of grain boundaries in these materials. It is established that superplastic deformation allowed not only to attain their efficient forming, but also to improve the ultrafine-grained structure and to obtain enhanced mechanical properties in the articles produced. The results demonstrate the possibilities of new applications of superplastic forming using bulk nanostructured materials.

Abstract: This work is devoted to enhancement of strength and ductility of the Ti-6Al-7Nb ELI alloy, which is less harmful from medical point of view for human body in comparison to Ti-6Al-4V. It has been demonstrated that formation of an ultrafine-grained structure in the alloy with the help of equal-channel angular pressing in combination with heat and deformation treatments allows reaching high strength (UTS = 1400 MPa) and sufficient ductility (elongation 10 %).

Abstract: This work presents the possibility of strength enhancement in the -alloy Ti-6.8Mo-4.5Fe-1.5Al via equal channel angular pressing at room temperature without precipitation of a secondary -phase. Influence of the initial structure of the alloy and ageing temperature on the density of precipitations and dimensions of the secondary -phase is revealed. It has been stated that combination of the solid solution treatment with the subsequent ECAP processing and final ageing is an effective way to achieve superior strength and ductility.

Abstract: The results of fatigue tests to determine the properties of commercially pure ultrafinegrained (UFG) Ti long-length rods processed by severe plastic deformation are presented. Fatigue tests were carried out on smooth and notched samples. It is shown that the formation of a UFG structure in Ti rods resulted in enhancement of the fatigue strength of smooth and notched samples.

Abstract: Ti-6Al-4V ELI (extra low interstitials) was processed by equal channel angular pressing in order to obtain an ultrafine-grained (UFG) microstructure which is known to enhance the fatigue behavior of metallic materials. Fatigue properties of UFG Ti-6Al-4V ELI were studied by strain and stress controlled fatigue tests. UFG Ti-6Al-4V ELI shows an improvement of the fatigue behavior compared to conventional grain (CG) size counterpart. Microstructural investigations prior to and after fatigue testing confirm a high structural stability of the UFG material. Hence, the UFG alloy has a high potential for prospective use in biomedical and engineering applications.