Papers by Author: Jae Hoon Lee

Abstract: he aim of this study was to evaluate the effect of HA on the demineralization resistance and bonding strength of light-curing glass ionomer dental cement. Tests were conducted using (1) pure Fuji II LC GIC, (2) 15% micro HA-Fuji II LC GIC. Physical properties, demineralization resistance and bonding strength to dentin of teeth were determined. The curing depth in all groups were satisfied the requirement of curing depth of ISO 9917-2:2004(minimum curing depth = 1mm). The depth of cure was reduced with addition of HA, presumably due to the light scattering effect of HA particles. Regarding sensitivity to ambient light, there were no detectable changes of the homogeneity in any groups. Also all groups were satisfied the requirement of the flexural strength of ISO 9917-2:2004(minimum flexural strength = 20MPa). 15% HA-Fuji II LC GIC group was found to present a greater flexural strength than pure Fuji II LC GIC, as the addition of HA promotes a chemical reaction between the HA, the glass powder, and the polyacid. Observing under the CLSM after 4 days of demineralization, there were significant differences in the CLSM and SEM images. Pure Fuji II LC GIC group showed greater enamel demineralization layer than in 15% HA-Fuji II LC GIC group. In SEM analysis, there was greater enamel demineralization in the pure Fuji II LC GIC group, and less demineralized under the influence of HA particles, 15% HA-Fuji II LC GIC group had more even surface particles. 15% HA-Fuji II LC GIC group was found to present a greater bonding strength than pure Fuji II LC GIC group. Observing the fractured surfaces under SEM after the bonding strength test, the cohesive failure rate was found to be in increasing order of pure Fuji II LC GIC, 15% HA-Fuji II LC GIC group. There were bone-like apatite particles observed to be formed in 15% HA-Fuji II LC GIC group.

Abstract: This study aimed to evaluate the anticariogenic and remineralization effects of the glass ionomer dental luting cement containing nano-β-TCP in vitro. The β-Tricalcium Phosphate (β-TCP) are the components of dental enamel and bone mineral as biological apatites. In addition, β-TCP contains a significant amount of calcium and phosphate, which can promote remineralization of enamel subsurface lesions in animal and human. RelyXTM glass ionomer cement(3M/ESPE, USA) was used as dental luting cement. Film thickness, setting time, and compressive strength was measured for each group of pure glass GIC, 15% nano-β-TCP GIC. Human molars were prepared in box-shaped cavities that were filled with the GIC with and without the 15% nano-β-TCP were placed in 25ml of pH 5.0 acid buffer for 4 days at 37°C. After 4 days, longitudinal sections (1007m) were obtained through the center of each restoration. The sections were analyzed using a scanning electronic microscope (SEM) and confocal laser scanning microscopy (CLSM) to identify the change in the enamel surface. A significant difference in the CLSM images between pure GIC and nano-β-TCP-GIC. CLSM allows the demineralized surface layers of sound enamel to be visualized down to approximately 100 μm. The pure GIC specimens had a relatively thick fluorescent layer. On the other hand, the fluorescent layer of the nano-β-TCP-GIC specimens were thinner. The SEM images of micro surfaces demonstrate that nano-β-TCP-GIC is less rough than pure GIC. Therefore, the addition of nano-β-TCP enhanced protection against acid demineralization and promoted remineralization of enamel surface.

Abstract: This study evaluated the marginal fit of CAD-CAM Zirconia cores with different proximal height. Thirty Zirconia cores and ten metal ceramics crowns were used to evaluate the marginal gap. The marginal fit was determined to be perpendicular to the tooth axis between the most apical point on the coping margin (core) and the reference marks on the mesial, distal, labial, and palatal surfaces of the die at several key stages of crown fabrication; before porcelain built-up, after body porcelain built-up, and after glazing. Additionally, an opaque stage for the metal ceramic copings was compared as well. Each measurement was carried out with a microscope. The means of gaps among the groups were 58±27 -m, 69±23 -m, 89±29 -m and 80±28 -m, groups I, II, III and IV, respectively. In relation to the proximal and labiopalatal surfaces there were no statistical difference among the groups, except group I. No significant differences were observed in firing stages of all groups. The findings of this study showed that the mean marginal gap of Zirconia cores with different proximal heights fell well within the acceptable clinical ranges.

Abstract: The mineral phase of bone and teeth is mainly hydroxyapatite. Currently there are numerous researches being conducted on the effect of the addition of hydroxyapatite to dental materials. Among them, several studied were published stating that the addition of hydroxyapatite to composite resin or glass ionomer cement resulted in an improvement in bonding strength and physical properties Therefore, this study will investigate the effect that the addition of hydroxyapatite to light curing glass ionomer cement has on bonding strength. Two different light curing glass ionomer cement products were selected (FujiⅡLC, GC Cor, Japan and Vitremer™ , 3M/ESPE, USA) and hydroxyapatite was mixed into the light curing glass ionomer cement at various concentrations to create hydroxyapatite-light curing glass ionomer cement mixture. In order to confirm that hydroxyapatite-light curing glass ionomer cement met the basic requirements of dental materials, sensitivity to ambient light, depth of cure, and flexural strength were tested. From the results of the above mentioned tests, the hydroxyapatite-light curing glass ionomer cement with the most superior physical properties for each product (15% HA-Fuji Ⅱ LC, 20% HA-Vitremer™)was bonded to the teeth and then immersed in artificial saliva(36.5°C) for four weeks. Finally the sectioned surface was observed under SEM after measuring the bonding strength. As the hydroxyapatite concentration increased, the depth of cure decreased. However flexural strength increased and there was not much change in the sensitivity to ambient light. Bonding strength, which was the main focus of this study, increased with the addition of hydroxyapatie and scanning electron microscope findings show a more cohesive type of fracture in the material with bone like apatite material formation along the tooth-material interface.

Abstract: A ceramic-polymer nano-hybrid, in which the bioactive silicate surface is nano-hybridized with flexible silicone bulk, was synthesized in the tetraethoxysilane (TEOS)-polydimethylsiloxane (PDMS) sol-gel system. Different solutions for surface silicate and bulk silicone, whose component ratio of SiO2: PDMS were respectively 100: 0 and 50: 50, were subjected to lamination and delayed polymerization and condensation process, producing a large transparent crack-free monolithic bulk. Characterizations at near-surface cross-section of the hybrid bulk revealed typical bioactive silicate structure with no distinct interface with the interior, indicating possibility of a novel bioactive nano-composite with enhanced physical and biological functions.