Papers by Author: Jiří Man

Abstract: Characteristic features of fatigue damage of 316L austenitic stainless steel cyclically strained axially in tension-compression, reversed torsion and combined axial-torsional mode were studied. All loading modes resulted in the formation of persistent slip markings (PSMs). Predominantly one slip system was activated in the case of axial and torsional loading while at biaxial loading, activation of several slip systems was involved. PSMs acted as sites of multiple fatigue crack initiation. The path of subsequent crack growth at a macroscopic scale differed considerably in dependence on loading mode and applied amplitude. The hardening-softening curves and fatigue life curves were evaluated and results were compared and discussed in terms of the type of applied loading.

Abstract: Atomic force microscopy (AFM) and focused ion beam technique (FIB) were adopted to study the early stages of surface relief evolution in 316L steel and polycrystalline copper fatigued with constant plastic strain amplitudes at different temperatures (316L steel at 93, 173 and 573 K; copper at 83, 173 and 295 K). Qualitative and quantitative data on the morphology and shape of persistent slip markings (PSMs), occurrence of extrusions and intrusions and the kinetics of extrusion growth are reported. They are discussed in relation with recent physically based theories of surface relief formation leading to fatigue crack initiation.

Abstract: Cyclic plastic straining in crystalline materials is localized to persistent slip bands (PSBs) and results in formation of persistent slip markings (PSMs) consisting of extrusions and intrusions. Intensive plastic strain in PSBs results in dislocation interactions and formation of point defects. The extended model based on point defect formation, migration and annihilation is presented describing surface relief formation in the form of extrusion-intrusion pairs. Point defect migration and resulting mass transfer is the principle source of cyclic slip irreversibility leading to crack-like defects - intrusions. Fatigue cracks start in the tip of sharp intrusions.

Abstract: Flat specimen of 316L steel was cyclically pre-deformed with constant plastic strain amplitude to early stage of fatigue life relevant to the period of cyclic strain localization and fatigue crack initiation. To document slip activity and reversibility/irreversibility of persistent slip bands (PSBs) in situ experiments in the high-resolution SEMFEG under special imaging conditions were performed. The half-and full-cycle slip activity and distribution of plastic strain within PSBs in individual grains were investigated via slip steps generated in half-and full-cycle deformation after intermediate vibration polishing. After completion of in situ tests the surface topography in identical locations was quantitatively documented using atomic force microscopy (AFM).

Abstract: Persistent slip markings (PSMs) were experimentally studied in 316L steel fatigued to early stages of the fatigue life. High resolution SEM, combined with focused ion beam (FIB) technique and atomic force microscopy (AFM) were used to assess the true shape of PSMs in their early stage of development. General features of PSMs in fatigued metals are extrusions and intrusions. Their characteristic features were determined. They were discussed in relation with the theories of surface relief formation and fatigue crack initiation based on the formation, migration and annihilation of point defects in the bands of intensive cyclic slip - persistent slip bands (PSBs)

Abstract: Smooth specimens made from austenitic-ferritic duplex steel were subjected to constant stress amplitude loading with positive mean stresses. Hysteresis loops were recorded during the fatigue life and plastic strain amplitude and cyclic creep rate were determined. Fatigue hardening/softening curves, cyclic creep curves and cyclic stress-strain curves for different positive mean stresses were evaluated. Typical dislocation structures developed in both phases of the duplex steel were identified using TEM, compared with the saturated plastic strain amplitude and correlated with the decrease of the cyclic creep rate during cycling and the slope of the cyclic stress-strain curve.

Abstract: Dislocations structures were studied using transmission electron microscopy in specimens of cast polycrystalline nickel based superalloy Inconel 792-5A cyclically strained up to failure with constant total strain amplitudes at temperatures 23 and 700 °C. Spatial arrangement of dislocations in individual grains was determined using the technique of oriented foils. Planar dislocation arrangements in the form of bands parallel to the {111} planes were observed in specimens cycled at both temperatures. The bands showed up as thin slabs of high dislocation density cutting both the γ channels and γ´ precipitates. They correspond to areas of cyclic slip localization. Experimental results concerning the dislocation structure are used to discuss the effect of temperature on the cyclic stress-strain response and fatigue life.

Abstract: Austenitic stainless steel was cycled at a series of temperatures in the interval from 296 K to 113 K. Constant plastic strain amplitude loading at different levels of plastic strain amplitude and testing similar to multiple step test method were applied at different temperatures. The stress amplitude was continually recorded and selected hysteresis loops were stored and later analyzed using statistical theory of the hysteresis loop. Effective stress component and probability density function as a function of temperature were evaluated. The results were discussed in terms of the temperature dependence of the cyclic yield stress and its sources.

Abstract: This numerical study focuses on the recent observations of Man et al. [4] showing welloriented grains presenting no Persistent Slip Marking even if PSMs are observed in 86% of the surface grains in 316L austenitic stainless steel cycled at room temperature up to 60% of fatigue life. Scanning Electron Microscopy (SEM) permits us to build Finite Element (FE) meshes of the observed aggregates and to assign to the modelled grains the crystallographic orientations measured by Electron Back Scattering Diffraction (EBSD). Then, 3D FE computations using crystalline elasticity allow the evaluation of mean grain stress tensors and resolved shear stresses. The results could explain qualitatively the anomalous behaviour of the studied well-oriented grains which is partly due to the particular orientations and shapes of the neighbour grains. This study highlights the influence of crystalline elasticity and neighbour grains in microplasticity and crack nucleation.

Abstract: Cyclic strain control tests have been performed on cylindrical specimens of cast polycrystalline Inconel 792-5A superalloy at 23, 500, 700 and 800 °C in laboratory atmosphere to study the effect of temperature on the fatigue behavior. Cyclic hardening-softening curves and fatigue life curves were measured. Scanning electron microscopy was used to investigate the surface relief. Low amplitude straining was characterized by saturation of the stress amplitude. In room temperature high amplitude straining cyclic hardening was followed by marked saturation. Pronounced continuous hardening until failure was observed at 500 °C. Initial cyclic hardening was followed by softening at 800 °C. A systematic shift of the Manson-Coffin and of the Basquin curves to lower fatigue lives was found when temperature was increased. Fatigue cracks were observed to initiate from surface slip markings at all temperatures.