Papers by Author: John J. Jonas

Abstract: Orientation-controlled copper bicrystals containing symmetrical 70o [0 0 1] tilt boundaries were deformed in tension at 923 K and at three initial strain rates from 4.2 x 10-5s-1 to 4.2 x 10-3s-1. The load was applied parallel to the grain boundary so as to eliminate grain boundary sliding. The nucleation of dynamic recrystallization (DRX) was investigated using optical microscopy and orientation imaging microscopy methods. After grain-boundary migration (GBM) and bulging, nuclei appeared behind the most deeply bulged grain boundary regions. The critical strain for nucleation was less than one-half of the peak strain and largely independent of the strain rate. At a fixed strain, nucleation is more frequent and the grain size finer as the strain rate is increased. All the nuclei were twin-related (Σ3) to the matrices. Furthermore, most of the twinning plane traces were parallel to the inactive slip traces of the bicrystals. This indicates that twin variant selection is essentially unaffected by dislocation motion. The observed mechanism of nucleation of DRX is discussed in relation to the occurrence of GBM and twinning.

Abstract: Two low carbon steels alloyed with 0.48wt% and 0.78wt% Cr were warm rolled to 65% reduction at 640°C. Annealing was carried out at 710°C to achieve a range of recrystallized volume fractions up to 100%. Texture analysis was performed by X-ray diffraction and Electron Back Scattering Diffraction. During the initial stages of recrystallization, more recrystallized grains nucleated at shear bands than at grain boundaries in the 0.48wt%Cr steel, whereas this was not the case in the 0.78wt%Cr steel. This is associated with a decrease in the propensity to form shear bands due to the lower amount of C in solid solution in the high-Cr steel. Additionally, the nuclei showed a preference to develop the same fiber as the deformed region within which they nucleated. In both steels, an increase in the annealing time led to the deterioration of the ND (or γ) –fiber and a strengthening of both the RD (or α) –fiber and Goss component. In the fully recrystallized samples, the ND component was somewhat stronger in the steel with the higher Cr content.

Abstract: The orientation relationships that apply to phase transformations in high-performance TRIP and TWIP steels were characterised by orientation imaging and EBSD techniques. The results are presented in the fundamental zones of Rodrigues-Frank space that correspond to the specific phase transformation under consideration (cubic to cubic or cubic to hexagonal). The use of Rodrigues-Frank space enables straightforward comparison to be made with orientation relationships proposed in the literature. The observations indicate that the active slip systems in the parent phase play important roles in variant selection.

Abstract: The kinetics of interpass softening and the strain (ε*) at which they become strain-independent were determined by means of double-hit hot compression tests. For this purpose, interrupted compression tests were conducted at strain rates of 0.01 and 0.1 s-1 to initial strains ranging from that corresponding to the initiation of DRX (εc) to the onset of steady state flow (εs.). Test temperatures between 1000 and 1100 °C (inclusive) were employed. Interpass times were varied from 0.3 to 1000 seconds. The fractional softening was determined using the 0.2% offset method. It is clear from the results that there is a transition strain (ε*) that separates the straindependent range of post-dynamic softening from the strain-independent range. The value of ε* obtained in this work was ε* = 4/3 εp. It was also found that the strain hardening rate was identical at all the critical strains (ε*) and took the value -22 MPa.

Abstract: Orientations of both the α and γ phases in a multi-phase commercial steel were measured by means of electron backscatter diffraction (EBSD) techniques. Using the average orientation of each austenite grain as the reference frame, the orientation relationships between the two lattices were compared with the common orientation relationships (i.e. the Kurdjumov-Sachs and Nishiyama-Wassermann) in Rodrigues-Frank space. The occurrence of variant selection in individual austenite grains was examined using a recent dislocation-based model. This model considers the role of the slip systems that were active during prior deformation, as well as those of in-plane reactions, cross-slip and the partial dislocations that are linked to specific variants. It also unites the competing K-S and N-W relationships through the dissociation of perfect dislocations. Reasonably good agreement was observed between the predictions and the observations. Possible explanations for some of the discrepancies are also presented.

Abstract: Experiments were carried out in which the dependence of the fractional softening on temperature, time and strain rate was determined in a 304H stainless steel. Three prestrain ranges were identified pertaining to three different post-deformation softening behaviors: 1) prestraining to below the DRX critical strain: strongly strain dependent softening by SRX alone with softening kinetics controlled by growth rate of the nuclei; 2) prestraining to above the DRX critical strain: SRX + MDRX softening with weaker strain dependence of the kinetics but still controlled by grain growth; 3) at a prestrain of ε* and beyond: nucleation-controlled MDRX softening with the full inhibition of SRX. The transition prestrain ε* can exceed the peak strain if the DRX grain refinement ratio g = D0/DDRX > 4. The transition to MDRX-dominated softening can be attributed to a constant value of the normalized strain hardening rate independent of the preloading temperature and strain rate. The softening data from the compression tests show that at ε*, the time for half softening t50 exhibits a minimum. These data differ somewhat from observations obtained in the torsion testing of solid bars, in which no strain dependence of t50 was detected at ε* and beyond. Whether or not the strain dependence of t50 vanishes in the MDRX range is sensitive to the test method employed to study the post-deformation softening.

Abstract: Superplasticity refers to a high temperature deformation process involving a marked sensitivity of the flow stress to the imposed strain rate, with resulting enhanced ductility. Although conventionally associated with fine-grained materials, superplasticity has recently been observed in coarse-grained alloys. The present research involves the deformation behavior of Al-Mg base alloys, where superpure Al-3%Mg and Al-5%Mg, and commercial Al 5056 were selected for study. The results for the Al-5%Mg and Al 5056 alloys are presented in this article. Flat sheet-type samples were tensile tested to 10% strain at increasing temperatures and at prescribed strain rates (0.001/s, 0.01/s, and 0.1/s). The dependence of flow stress on temperature was found to display some unusual characteristics. This behavior is interpreted as resulting from the occurrence of dynamic strain ageing (DSA). The aim of the overall study is to determine the relation between DSA and superplasticity in coarse-grained Al-Mg alloys. This will, in turn, lead to the control of the strain ageing behavior so as to produce the largest possible values of strain rate sensitivity (and, hence, elongation).

Abstract: Research is currently being conducted on the feasibility of hydroforming extruded magnesium tubes to integrate multiple parts into a single hydroformed section. Among other applications, such sections would reduce the weight of both cars and planes, particularly when used in the vehicle frame. This would lead to either reduced fuel costs, or the ability to carry an increased payload. Magnesium generally has limited ductility, which in the case of the current extruded tubes is even further reduced at the extrusion seams. These are locations where the material flow separates and rejoins during extrusion and are unavoidable when a hollow profile die is used. When the tubes were stressed in a circumferential direction, tube ruptures consistently occurred along the extrusion seams of the tubes. This led to the current project, an inquiry into the exact cause of failure at these locations. The creation of irregularities at the seams, such as precipitate dispersions, local texture changes, grain size changes and entrained material, is discussed. These irregularities are considered together with their roles in producing the failures. The results are summarized and the most fruitful directions for future work are outlined.

Abstract: The influence of chromium and phosphorus addition on the microstructure and on texture development was studied during the early stages of the annealing of warm rolled, low carbon steels. The addition of alloying elements led to an increase in the volume fraction of grains containing both shear bands and microbands. Moreover, the alloyed steels displayed lower stored energies and dislocation densities compared with an unalloyed low carbon steel. Two types of carbides were present after warm rolling in the steels containing the alloying additions: (i) coarse carbides; and (ii) fine strain-induced particles. These microstructural differences affected the development of texture during annealing.

Abstract: In warm rolled steels, the intensity of the <111>//ND annealing texture, which favours formability, has been related to the formation of shear bands during rolling. Coarse hot band grain sizes (HBGS’s) facilitate flow localization, the mechanism associated with the formation of shear bands.In this work, the effect of grain size after hot rolling was studied in a low carbon steel containing small additions of Cr and Mn. The formation of shear bands and their subsequent influence on the normal anisotropy rm and planar anisotropy Dr in the annealed steels were of particular interest. Two HBGS’s (18 and 30mm) were employed and the specimens were warm rolled to reductions of 65 and 80% at various temperatures between 640 and 700°C. The results show that the frequency of shear banding is slightly lower for the smaller grain size. The normal anisotropy was not affected by the HBGS; by contrast, much lower Dr values were associated with the finer grained steel.