Papers by Author: Liang Zuo

Abstract: In this paper, the texture and micro-orientation of FSS (Ferritic Stainless Steel) during hot rolling, cold rolling and annealing were studied by using x-rays and EBSD technology. The results shown that as cast ingot of FSS was compose of random orientations equiaxed grains and <001>∥ND columnar grains; after hot rolling, the preferred orientation of <001>∥ND columnar grains of as cast ingot obtained inherits, the fiber texture was obvious stronger than that of equiaxed grains; during cold rolling, the initial <001>∥ND columnar grains turn to  fiber texture,  fiber texture can not be found.

Abstract: In this paper, we report some ab initio calculation results of three perfect stoichiometric alloy systems Ni2XGa (X = Mn, Fe, Co). The calculations have been performed on optimizing the crystal structures in both austenitic and martensitic phases, the electronic density of states (DOS), the magnetic properties and the difference of charge distributions on considering that Mn, Fe, Co are adjacent to each other within one period in the periodic table of elements, and they are all ferro-magnetic. We have shown the impact of these magnetic elements on several properties of each alloy. Study on these three Heusler alloy systems is important in view of property prediction.

Abstract: In the present work, we summarize three calculation methods to determine some specific crystallographic elements based on electron diffraction orientation measurements by SEM and TEM. The first one is to determine the plane indices of the faceted interfaces where the orientation relation¬ships (ORs) between the adjacent crystals are reproducible. To acquire the orientation data, we need to prepare only one sample surface but not two perpendicular sample surfaces as usually required in the standard double trace method. The second is to characterize the surface crystalline planes and directions of a faceted nano-particle under TEM imaging and diffraction mode. With the determination of the edge trace vectors and then the plane normal vectors in the screen coordinate system of TEM, their Miller indices in the crystal coordinate system can be calculated through coordinate trans¬formation. The third method is to determine the twin type and the twinning elements based on the orientation information acquired by SEM EBSD measurements from the two twinned crystals through misorientation calculations. These methods will facilitate related studies.

Abstract: Intergranular exchange coupling between magnetic nano-grains is one of important parameters to develop magnetic recording media towards the areal density of 1000 Gbits/in2. In this presentation, various processings, involving oxide co-sputtering for perpendicular media, spontaneous phase separation for longitudinal media, and grain boundary (GB) diffusion derived from underlayer or overlayer to induce tunable exchange coupling, have been reviewed to tailor the exchange coupling, including their main principles, present achievements and engineering challenges. Much attention is paid to the physical origin of magnetically induced phase separation of Co-Cr-based alloy, which governs media noise and coercivity, and its applications to the longitudinal media. A proposal of GB diffusion is also highlighted in detail to show a feasibility to tailor the exchange coupling, including calculation results and experimental evidences.

Abstract: An AC magnetic field (0.5Tesla) is applied with the field direction perpendicular to the rolling direction during annealing of a 76% cold-rolled IF steel sheet. Microstructure and texture evolution in the as-annealed specimens were determined using SEM based OIM technique. It is found that the recrystallization is noticeably retarded by AC magnetic field annealing. At the early stage of recrystallization (annealing at 650°C for 30min), the development of (111) <123> orientations was favored by the AC magnetic field. With progress of recrystallization (annealing at 700°C and 750°C for 30min), the applied AC magnetic field suppressed the development of γ-fiber recrystallization textures to some extent.

Abstract: The effect of high magnetic field annealing on the nucleation sites for recrystallized nuclei with {111}<112> orientation in the initial stage of recrystallization in as-annealed interstitial-free (IF) steel sheet were investigated by the SEM-EBSD analysis. Specimens of cold rolled IF steel sheet were annealed at 650°C for 0min and 10min respectively with a 12-tesla magnetic field to obtain a partially recrystallized microstructure. During the magnetic field annealing, they were respectively placed at the center of the applied field with their rolling planes parallel to the magnetic field direction (MD), and with their rolling direction (RD) parallel and normal to the MD, respectively. It was found that different to the non-field annealed specimen, in the field annealed specimens, the {111}<112> oriented recrystallized nulei favored to nucleate in the {111}<112> deformed matrix and not in the {111}<110> deformed matrix. This phenomenon may be attributed to the magnetic ordered state induced by the magnetic field, which might suppress the formation of high-energy grain boundaries between the newly formed nuclei and the deformed matrix.

Abstract: The texture, the formability and the correlation between formability indices of Al-0.9Mg- 1.0Si-0.7Cu-0.6Mn alloy for automotive body sheets subjected to solid solution, T4, annealing treatment and artificial aging at 443k for different time were investigated by orientation distribution functions(ODF) analysis, tensile and cupping test, FLD measurement and regression analysis method. The results showed that the textures of cold rolled alloy sheets consist mainly of copper and brass orientations, which are transformed into the texture mainly containing {001}<310> orientation after recrystallization, and aging treatment has little influence on the recrystallization texture. The formability of alloy sheets subjected to solid solution, T4 and annealing treatment is similar, however, the formability was observably deteriorated after aging at 443k. The correlation between uniform elongation δu and FLD0 is the most remarkable in all the given formability indices, the correlation between strain-hardening exponent n and the FLD0 take second place, while there is no correlation between plastic strain ratio r and FLD0. The correlation between reduction of area ψ and cupping value IE is distinct, while ψ and IE have little correlation with FLD0.

Abstract: In this paper, some of our recent results in phase equilibrium, microstructure, texture and precipitation resulting from the application of an external high magnetic field during diffusional phase transformation in both medium carbon and high carbon steels have been summarized Their potential engineering applications are foreseen.

Abstract: The hot bands of non-oriented electrical steel were cold rolled by asymmetric rolling with speed ratio of 1.125 as well as conventional symmetric cold rolling to investigate the effects of cold rolling mode on through-thickness texture variation. Asymmetric rolling shows a marked weakening effect on α fiber (RD//<110>) running from {001}<110> to {112}<110> through sheet thickness, especially at the side contacting with faster roll. Asymmetric rolling increases {111}<112> component while decreases {111}<110> component through sheet thickness except for the surface layers. The through-thickness texture variation due to asymmetric rolling was explained in terms of shear strain distribution.

Abstract: High-energy synchrotron diffraction offers great potential for experimental study of recrystallization kinetics. A fine experimental design to study the recrystallization mechanism of Interstitial Free (IF) steel was implemented in this work. In-situ annealing process of cold-rolled IF steel with 80% reduction was observed using high-energy X-ray diffraction. Results show that, the diffraction intensity of {001}<110> and {112}<110> belong to α-fiber texture component decreased with the annealing temperature increased while {111}<110> did nearly not change and {111}<112> increased; the FMTH decreasing and d-space changing with annealing temperature increasing indicated that the residual stress relaxed completely during recovery.