Papers by Author: Lorella Ceschini

Abstract: This study focuses on the role of Mo addition on the mechanical properties of an Al-Si-Cu-Mg alloy in as-cast and heat-treated condition at ambient and elevated temperature. Addition of 0.4 to 0.6 wt.% Mo forms Mo-bearing dispersoid particles which have a relatively high melting point and improve high temperature tensile strength. Ductility suffered in the presence of Mo-bearing particles. Trace addition of Mo up to 0.6 wt.% has a negligible influence on the yield strength and hardness of Al-Si-Cu-Mg alloy in as-cast and heat-treated conditions at ambient temperature and 250 °C.

Abstract: Al-Si-Mg alloys are commonly employed for the production of automotive castings. In view of the recent stringent emissions standards and consequent engine downsizing, these components must withstand higher temperatures and stresses than in the past. In this regard, the heat treatable quaternary Al-Si-Cu-Mg alloys gained particular interest in recent years, due to their superior mechanical properties and higher thermal stability. The present research activity was addressed to evaluate the influence of cooling rate on microstructure and consequently on room temperature tensile and fatigue behaviour of the A354 and C355 alloys. Samples for mechanical tests were produced under controlled cooling rates, in order to induce different secondary dendrite arm spacing (SDAS) values, classified as fine (20-25μm) and coarse (50-70μm). The experimental results showed that the cooling rate strongly influences the type, size and morphology of intermetallic particles. The presence of coarse intermetallic phases, mostly Fe-based, observed in coarse SDAS specimens, was reported to strongly affect ultimate tensile strength (UTS), elongation to failure and fatigue strength of both the investigated alloys. A correlation between UTS and fatigue resistance was found, independent of microstructural coarseness.

Abstract: The high temperature tensile behaviour of the A354 casting aluminum alloy was investigated also evaluating the influence of secondary dendrite arm spacing (SDAS). Cast specimens were produced through a gradient solidification equipment, obtaining two different classes of SDAS, namely 20-25 µm (fine microstructure) and 40-50 µm (coarse microstructure). After hot isostatic pressing and T6 heat treatment, the samples underwent mechanical characterization both at room and high temperature (200 °C). Results of tensile tests and hardness measurements were related to the microstructural features and fractographic characterization, in order to investigate the effect of microstructure and high temperature exposure on the mechanical behaviour of the alloy.

Abstract: The present study aims at producing Al-based nanocomposites reinforced with low fractions of ceramic nanoreinforcement produced by thermal plasma, evaluating the strengthening effects induced by their addition to the widely used A356 (Al-Si-Mg) cast aluminum alloy. Nanoparticles were produced using a lab-scale RF inductively coupled thermal plasma system designed by simulation as to optimize the plasma operating conditions and reactor geometry. During the casting route, ultrasonic treatment of the melt was performed to better disperse the reinforcing particles into the matrix. Ceramic spherodized microparticles were also synthesized and micro-reinforced Al-matrix composites were produced with the same route for comparison. Microstructural characterization of the cast samples was carried out by optical and scanning electron microscopy (SEM) with energy dispersive spectroscopy (EDS) analysis. BET analysis was also used for powder characterization. Hardness tests were performed to assess the enhancement in mechanical properties obtained by addition of nanoparticles with respect to both the microparticle reinforced and unreinforced Al-Si-Mg matrix.

Abstract: The aim of the present study was to characterize the high temperature tensile behaviour of the C355 (Al-Si-Cu-Mg) alloy produced under controlled casting condition so as to obtain different secondary dendrite arm spacing (SDAS). C355 samples were produced through a gradient solidification equipment able to produce microstructures with fine (20-25 μm) and coarse (50-70 μm) SDAS values. The as-produced specimens were subjected to hot-isostatic pressing and then T6 heat treated. Microstructural characterization, room and high temperature (200 °C) tensile tests were carried out on the heat treated specimens. The tensile behaviour was related to the different SDAS value of the samples.

Abstract: The widespread use of metal matrix composites (MMC) is often limited due to the difficulties related to their joining by means of traditional fusion welding processes. The aim of this work was to evaluate the effect on microstructure and mechanical properties (hardness and tensile strength) of two different friction welding techniques used for joining two Al-based metal matrix composites. In particular, Friction Stir Welding was applied to a 6061 (Al-Mg-Si) alloy matrix, reinforced with 20vol.% of Al₂O₃ particles (W6A20A), while Linear Friction Welding was applied to a 2124 (Al-Cu-Mg) alloy matrix reinforced with 25vol.% of SiC particles (AMC225xe). Both the welding processes permitted to obtain substantially defect-free joints, whose microstructures was found to be dependent on both the initial microstructure of the composites and the welding processes. Hardness decrease was in the order of 40% for the FSW joint and of 10% for the LFW joint, mainly due to overaging of the matrix induced by the frictional heating, while the joint efficiency in respect to the ultimate tensile strength was 72% and 82%, respectively. Elongation to failure increased in the FSW joint due to coarsening of precipitates, whereas it decreased in the LFW joints due to the fibrosity in the thermomechanically altered zone. Fracture surface analysis showed good matrix/reinforcement interface for both composites.

Abstract: The present study focuses on the influence of the PEO (Plasma Electrolytic Oxidation) treatment on the tribological behaviour of the AA2618/20 % vol. Al₂O₃p composite, dry sliding against induction hardened UNI C55 steel. Particle-reinforced Al based composites offer a higher wear resistance by comparison with the corresponding unreinforced alloys, however, the presence of critical loads and/or velocities which lead to transition towards severe wear regime, was often observed. In such conditions, the composite can show higher wear rates than those of unreinforced alloys. For this reason, surface modifications, such as PEO, might contribute to improve wear resistance. In this paper, topography, microstructure, phase constitution and surface hardness of the PEO-treated composite were investigated and its tribological behaviour was studied by dry sliding tests using a block-on-ring tribometer. The results were compared with those from the uncoated composite, demonstrating a very positive effect of the PEO treatment, which moved transitions from mild to severe wear towards more severe test conditions, in terms of both load and velocity.

Abstract: This paper presents the results of microstructural and mechanical characterization of Friction Stir Welding joints of two aluminum-based particles reinforced composites. The composites were FSW in the extruded and T6 heat treated condition. No post-weld heat treatment was carried out on the FSW joints. Hardness, tensile, low-cycle fatigue and impact tests were carried out. Microstructural and fractographic characterization were performed both on the base and FSW material, in order to investigate the effect of the solid-state welding process on the reinforcement particles and aluminum matrix. The FSW produced high quality joints with good microstructural characteristics: the welded zone displayed a refinement of the Al matrix grain size and reinforcement particles, and a better particle distribution. The FSW specimens showed high efficiency, both in the tensile, impact and fatigue tests.

Abstract: The aim of the present work is to evaluate the possibility of using the Linear Friction Welding (LFW) technique to produce similar and dissimilar joints between a 2024 Al alloy and a 2124Al/25vol.%SiCP composite. In this solid state joining process the bonding of two flat edged components is achieved through frictional heating induced by their relative reciprocating motion, under an axial compressive force. Microstructural characterization of the welds was carried out by optical and scanning electron microscopy, to investigate the effect of LFW both on the aluminium alloy matrix and the reinforcement particles. The mechanical behaviour of the welded specimens was studied by means of hardness and tensile tests. The mechanisms of failure were investigated by SEM analyses of the fracture surfaces. LFW joints in MMCs resulted substantially defect free, with a uniform particle distribution, while a partial lack of bonding at the corners was observed in the others welds. The hardness decreased by approximately 10% in the welded zone, with some data fluctuations due to the complex microstructural modifications introduced by the LFW process. The joint efficiency, evaluated in respect to the UTS, was 90% for the Al alloy joints and 80% for the MMC joints. A decrease in the elongation to failure was measured in all the LFW specimens, probably related to the orientation of the plastic flow in the TMAZ, where the fracture generally occurred.

Abstract: In the present study, the process modelling of AMCs linear friction weldment was carried out. Four major stages of the process (Part 1: Warm-Up; Part 2: Osci-Forging; Part 3: Forging; Part 4: Cool-Down) were identified and simulated consecutively to generate the temperature field and residual strains distribution within the model. An eigenstrain model calibrated by the neutron diffraction results was also employed to capture the permanent deformation distribution. Good agreement between the process modelling and the experimental measurements was found.