Authors: Mohamed Soliman, Adel Nofal, Heinz Palkowski
Abstract: Three ductile irons with different aluminum-and manganese-content were subjected to two thermo-mechanical schedules. In the first schedule, a total deformation of φt = 0.3 is applied on the ductile irons in the austenitic region before the austempering process. In the second schedule, the materials are subjected to deformation of 0.2 in the austenitic region and deformation of 0.1 during austempering (ausforming). Mechanical deformation of austenite prior to the transformation “stage I” pronouncedly accelerated the transformation due to increasing the nucleation sites of ausferrite. This increase has its impact on enhancing the microstructural uniformity and refining the ausferrite platelets. On the other hand, the retained austenite content was not significantly affected by the applied ausforming. Remarkable increase in hardness, strength and ductility of the ausformed ductile iron due to the latter effects is observed.
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Authors: Mohamed Soliman, Heinz Palkowski
Abstract: Microstructure evolution and tensile properties were studied in a bainitic pipeline steel grade by performing a number of physical simulations on samples machined out of an industrially produced transfer bar. In these simulations, the cooling interval between roughing and finishing stages (tV) was varied from 5 s to 180 s. The austenite status after this cooling interval, regarding the prior austenite grain size and precipitates, simulates the condition of austenite before entering the finishing mill. The finishing parameters and the subsequent cooling strategy were kept unchanged throughout all the applied simulation processes. The gradual increase in tV resulted in a gradual increase of the granular bainite phase on the expense of the aciculare ferrite. This resulted in an incremental decrease in ultimate tensile strength and yield strength with increasing tV. However, this behavior approached a steady state condition after which the tV has limited/insignificant effect on the ultimate-and yield strength. This saturating value of tV is process parameter dependent.
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Authors: Mohamed Soliman, Heinz Palkowski, Adel Nofal
Abstract: Using thermo-mechanical simulator equipped with dilatometry system, two ductile iron alloys with different Mn-content are processed by combining both, well defined deformation process and subsequent controlled cooling in a single processing chain to control the final microstructure. Accordingly, ductile irons with four different structrues are produced namely, martensite, ausferrite, martensite+ferrite and ausferrite+ferrite. Depending on the dilatometric measurments, the ferrite formation temperature-range has been defined for both alloys. Preferential transformation of austenite to ferrite at graphite nodules during cooling is observed. It is also observed that the formation of ferrite during cooling results in both decreased martensite start of the undecomposed austenite and accelerated kinetics of ausferrite formation.
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Authors: Mohamed Soliman, Mehdi Asadi, Heinz Palkowski
Abstract: Dilatometric measurements were used to design the processing parameters of two types of bainitic steels. The first type is a hypoeutectoid ultra fine bainite steel, for which the dilatometer was used to locate the temperature at which cementite is completely dissolved during intercritical annealing (TC). The intercritical annealing temperatures are then selected will above TC. To obtain the martensite start temperatures (MS), the steel is quenched to the room temperature (RT) from these selected temperatures and then the bainite transformation temperatures were selected to be well above MS. The dilatometer was then used to monitor the bainite transformation kinetics from which the required time frames for cessation of the bainitic reactions were estimated.
In the second type, bimodal bainite had been produced in thermo-mechanically processed TRIP-steel. A deformation dilatometer is used to perform three deformation-steps before slow cooling to form approx. 30% polygonal ferrite. The material was then rapidly cooled to the first bainite formation temperature. During this step, the dilatometer was used to monitor the bainite reaction from which the required time for 50% decomposition of austenite is estimated. The martensite start of the undecomposed austenite was located by quenching to RT. The second bainite transformation step was then performed well above the new MSII to form a second generation of finer bainite.
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