Papers by Author: R.M. German

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Abstract: Austenitic Stainless Steel Has a FCC Structure at Room Temperature and the Temperature Range of the Austenite Phase Depends upon its Composition. 316L SS Is Widely Used in Medical, Marine, Industrial, Sporting and Aerospace Applications due to its Excellent Combination of Mechanical Properties and Corrosion Resistance. this Study Presents the Defects Observed during Optimization of the Processing Parameters for the Fabrication of Powder Injection Molding (PIM) of 316L SS Parts. in this Study, Five Formulations of Feedstock Containing 60-71vol% of Metal Powder Were Prepared Using a Wax-Based Binder. Green Samples Were Injection-Moulded, Followed by Binder Removal by Solvent and Thermal Means. Paraffin Wax (major Binder) Was Extracted at Various Temperatures in Order to Determine the Solvent Extraction Temperature. the Thermal De-Binding Was Performed Successfully at a Temperature of 450°C by Varying the Heating Rate from 1°C/min -10°C/min. SEM Results Showed Complete Removal of the Plastic Binder. Test Samples Were Sintered at Various Temperatures and Atmospheres. the Defects Observed during Solvent Extraction Were Swelling, Cracks and, at the Thermal De-Binding Step, Collection of Binder, Swelling and Holes. Sintered Samples Showed a Loss of Dimensional Control. these Types of Defect Were Considered to Be due to Inappropriate Heating Rates, Temperature and Dwell Time at each Process Step.
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Abstract: This research presents the effects of temperature and cooling rate on mechanical properties of powder injection molded 316L Stainless steel. Steel powder and binder were mixed together to produce the feedstock. The green samples were produced by injection molding and debinded. Brown test samples were sintered in vacuum at 1325°C, 1360°C and 1380°C for 2h with two heating and cooling rates 5°C/min and 10°C/ min. The test samples sintered at 1325°C achieved maximum sintered density. The higher cooling rate improved the strength of the sintered test samples. The maximum sintered density of 96% and tensile strength of 503MPa was achieved and these results are comparable to the wrought 316L stainless steel (according to ASTM standard).
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