Papers by Author: Rinat V. Safiullin

Abstract: Nickel-iron Alloy 718 is widely used for fabricating parts by superplastic deformation. Refinement of grains down to a nanostructure (NS) size improves the alloy’s processing properties. Thermomechanical treatment has been carried out to form a NS state in bulk alloy by multiple isothermal forging (MIF) at gradually decreasing temperatures. Investigation of superplastic properties and processing behavior of Alloy 718 has been performed. The alloy with a grain size of 80 nm displays superplasticity (SP) at a temperature which is lower than for a conventional fine grained alloy by about 350°C. The values of the relative elongation  and the strain rate sensitivity coefficient m are 350% and 0.37, respectively. The experimental data on the influence of grain size on solid-state weldability in the range of SP have been obtained. The application of the effect of low temperature SP yields lower temperatures of superplastic forming (SPF) and pressure welding (PW) as compared with conventional SP of fine-grained material. The experiment of the combined process of SPF and PW by counter-forming of two polished sheets, demonstrates its low temperature processing feasibility using NS specimens. The SPF processing of NS sheets in a cylindrical die has been investigated. It has revealed that macro-deformation is uniform in cross and longitudinal sections. Mechanical properties of Alloy 718 in NS condition and after strengthening heat treatment have been discussed.

Abstract: A critical analysis of approaches to find constitutive relations from the tests on uniaxial and two axial loading is presented. Then we report on the methodology of fitting parameters of constitutive relations for superplastic forming based on the results of cone cup and elongated wedge cup tests. Optimal cone and wedge angles are estimated analytically and also from the results of finite element simulations. Our methodology is based on comparison of the experimental results and the results of numerical simulations of the corresponding tests in frame of the commercial software such as ANSYS10.0 (ED). We carry out numerical simulations of the cone cup and the wedge cup tests for different sets of parameters of the chosen constitutive relation and different values of friction coefficient in order to reproduce the experimental results. The parameters corresponding to the best fit of the experimental data are then recommended for the use in computer simulations of the superplastic forming of commercial products.

Abstract: Mechanical properties of a Ti2AlNb-based intermetallic alloy both at room and elevated temperatures were considerably improved due to formation of a homogeneous microstructure with the average grain size of about 300 nm. At room temperature, elongations up to 25% were obtained and the ultimate strength reached 1400 MPa. The alloy exhibited superplastic behavior in the temperature range of 850-1000°C. The maximum elongation of 930% and steady state flow stress 50 of about 125 MPa were obtained at 900°C and strain rate of 4.210-3 s-1. The nanostructured material was used for production of intermetallic sheets and multilayer composite plates consisting of alternating layers of orthorhombic intermetallic and commercial high temperature titanium alloy. Ti2AlNb-based sheets and composites exhibited improved mechanical properties.

Abstract: The as-cast and hot worked microstructures of the newly developed β-solidifying ingot-metallurgy Ti-45Al-X (Nb,Mo,B) alloy and its superplastic properties in the hot worked condition have been studied. The obtained experimental findings were used for research of superplastic forming and diffusion bonding of sheet products, which were cut out of hot worked preform by spark cutting. It was shown that superplastic forming might be successfully applied to the obtained fine-grained sheet materials. Relatively low bonding temperatures and pressures were found to be sufficient to achieve sound joints in the sheet material.