Authors: Feng Huang, Rui Run Chen, Jing Jie Guo, Hong Sheng Ding, Yan Qing Su, Heng Zhi Fu
Abstract: Effects of parameters on the stability of silicon melt pool in cold crucible continuous casting were discussed. The results indicate that the extinguishing of induction heating is mainly caused by the side wall feeding, low superheat degree and volume of the pool. The hot melt splashes are caused by the higher input power and uncompletely melted silicon of the dome top surface. The pool was shown to be stabilized as the raw materials were fed in the center area of the dome surface, the superheat degree and volume of the pool were properly increased, the pool was controlled in the effective heating range of the coil and the input power was set properly
771
Authors: Rui Run Chen, Jie Ren Yang, Hong Sheng Ding, Jing Jie Guo, Yan Qing Su, Feng Huang, Heng Zhi Fu
Abstract: In this study, Ti46Al0.5W0.5Si ingots were directionally solidified by a near-rectangular cold crucible under different process parameters. These process parameters include the electromagnetic stirring, the crucible configuration and the molten drop, all of them have important effect on the S/L interface. The effects of the parameters on the solid/liquid (S/L) interface morphology were investigated, and the mechanisms of the parameters influencing the S/L interface were discussed and revealed. Results showed that the typical S/L interface of the ingots was presented as a curved ‘W-type’ shape. The uneven temperature distribution in the front of the solidified interface is the main reason for a curved S/L interface. Further, the requirements for obtaining a planar S/L interface in the process of cold crucible directional solidification were given, which provided a guide for the future work.
767
Authors: Feng Huang, Rui Run Chen, Jing Jie Guo, Hong Sheng Ding, Yan Qing Su, Jie Ren Yang, Heng Zhi Fu
Abstract: A square shaped silicon ingot was cast by cold crucible continuous casting. The grain growth behaviors during different growth stages were investigated. In the first, grains nucleate at the base surface in the centre and in the three phase junction at periphery, and then grow upwards and inclined upwards separately. In the second, grain grow competitively, two distinguished zones are formed. In the final, a cap is formed on the liquid free surface, and precipitates are present.
398
Authors: Rui Run Chen, Hong Sheng Ding, Jing Jie Guo, Yan Qing Su, Heng Zhi Fu
Abstract: The ingot of Ti47Al alloy was prepared by a newly developed rapid directional solidification, the microstructure and compressive properties of the ingot was observed and tested. The results show that the macrostructure consisted mainly of coarse columnar grains parallel to the axial direction, with the size of 0.5mm wide and 10mm in length. The direction of lamellar is almost perpendicular to the growth direction in the longitudinal section and no dendritic core is found. The average ultimate compressive strength of the specimens with grain growth parallel/perpendicular to the compressive direction is 1233.3 and 861.7 MPa respectively. The fracture mode for specimens with grain growth parallel to the compressive direction exhibits predominantly translamellar fracture, however, that for specimens with grain growth perpendicular to the compressive direction exhibits predominantly delamenation or interlamellar fracture.
217
Authors: Feng Huang, Rui Run Chen, Jing Jie Guo, Hong Sheng Ding
Abstract: The electromagnetic continuous pulling is a newly growth technology as a promising process for silicon preparation, start-up heating is necessary for the semiconductivity of silicon at room temperature. Investigations were carried out to study this process in a square crucible with the frequency of 50kHz, details of the experimental procedure were given, the affecting factors, electrical performance and heat explosion problems during the process were measured and discussed. The results indicated that the best conditions for the preheating were the central position of the base in the coil, the higher power and the proper primary mass of silicon setting. The electrical performance indirectly showed the pool conditions and so it can be effectively used to control the melting operation.
756
Authors: Jie Ren Yang, Rui Run Chen, Hong Sheng Ding, Jing Jie Guo, Heng Zhi Fu
Abstract: This paper has systematically studied the evolving process of column crystals of Ti46Al0.5W0.5Si alloys that is directionally solidified by rectangular cold crucible. The results showed that: the solid/liquid interface presented convex to the liquid metal due to the complicated influences by cold crucible. Overheating temperature and new crystal nucleus had great effects on the growth continuity and the stability of column crystals. Furthermore, the precipitation phases have been studied. As a result, the methods for controlling growing process of columnar crystals have been submitted, which are playing a critical role in optimizing experimental parameters and devising the construction-elements of cold crucible.
743
Authors: Hong Sheng Ding, Rui Run Chen, Yan Li Wang, Heng Zhi Fu, Jing Jie Guo, Wei Sheng Bi, Jun Jia
2575