Papers by Author: Stefan M. Knupfer

Abstract: Residual strains in plasma sprayed and heat-treated hydroxyapatite (HA) coatings deposited on a titanium alloy (Ti-6Al-4V) substrate were investigated by means of neutron diffraction. Strain measurements were performed in vertical scan (“z-scanning”) mode to provide a through thickness strain profile in the coating and substrate materials. Results are discussed in terms of the influence of heat-treatment on the residual strain profile of these biomedical coatings. This investigation concluded that the heat-treatment had a significant effect on the residual strain profile in HA coatings.

Abstract: Forming of metal plates with a high-power laser beam is a flexible materials forming technique. Bending results from the establishment of a steep temperature gradient through the material thickness which leads to non-uniform thermal expansion/contraction and subsequently residual stresses. It is important to characterize these residual stresses as a function of process parameters such as line energy (LE) to optimize treatment conditions and to gain an insight into the mechanism of the formation of the final geometries. Non-destructive neutron diffraction measurements were carried out on ENGIN-X at ISIS and KOWARI at ANSTO to map the residual stress distribution around the heat affected zone (HAZ) of laser deformed mild steel plates for single and multiple passes as a function of line energy (LE), the primary laser forming process parameter. It was found that in the centre of the HAZ, longitudinal residual stresses are tensile and dominant, transverse stresses are predominantly tensile and normal stresses are compressive and close to zero. The residual strain in longitudinal direction increased with LE and number of passes until yielding. Even higher heat input decreased the magnitude of the cusp, but not its total height. The comparison of a stress-free reference sample, measured at both facilities, showed a small discrepancy in the lattice spacing corresponding to ~ 85 μstrain which is insignificant with respect to the experimental values measured.