Papers by Author: Stefano Amadori

Abstract: This work describes the anelastic behaviour of human dentin in the temperature range from 100 K to 673 K. Human molars, extracted from individuals (males 55-70 years old) as part of their dental treatment, were cut to obtain bar-shaped samples for mechanical spectroscopy (MS) experiments. The results are presented and discussed in two parts referring to experiments above and below room temperature.

Abstract: The work describes the anelastic behaviour of human dentin below room temperature. Human molars, extracted from individuals as part of their dental treatment, were cut to obtain bar-shaped samples for mechanical spectroscopy (MS) experiments. Repeated cooling-heating cycles in the range 300-100 K have been carried out on the same samples. In the cooling stage of the first cycle Q^-1 exhibits a very broad maximum due to a series of phase transformations involving water present in the pores, in the interstices between fibres, between fibrils and inside collagen triple helix. The formation of ice I_h produces permanent damages to the dentin structure (rupture of fibres and fibrils) leading to a decrease of maximum intensity in the following cycles. In the heating stage of all the cycles two maxima, M1 and M2, have been observed around 155 K and 178 K. M1 is due to the transformation of low-density amorphous (LDA) ice into ice I_C while M2 to that of ice I_C to ice I_h. Above 200 K, Q^-1 progressively increases with lower damping values in the cycles after the first one. Dehydrated samples do not exhibit the aforesaid anelastic phenomena confirming that their origin is connected to water and its transformations.

Abstract: Composites made from compacted powders blends of Al with different Fe contents were produced and characterised with respect to mechanical and induction heating properties. Mechanical spectroscopy and hardness measurements were employed to follow the evolution of Young modulus and internal friction after ageing. It was found that above a critical iron content (>30% of the volume) a percolation network of Fe grains is obtained inside the specimen and the induction heating characteristics become comparable with those of ferritic steel samples.

Abstract: Mechanical spectroscopy was employed to investigate the microstructure evolution of a Zr-modified 6082 Al-Mg-Si alloy and the same alloy with Sc addition after ageing and following severe plastic deformation through equal channel angular pressing. Measurements of the internal friction and dynamic young modulus have been performed in isothermal and isochronal runs in the frequency range 0.1 - 104 Hz. The anelasticity spectra reveal in the temperature range 470-870 K both structural and anelastic relaxation processes. Two structural damping maxima connected with inverse temperature trend of the modulus occur in the alloys submitted to equal channel angular pressing, the first one is strongly suppresed by Sc and Zr addition. An anelastic relaxation peak whose strength depends on the nature and morphology of precipitates and dispersoids and on the deformation and ageing condition was observed in all samples investigated. The high background damping occurring before the first structural damping maximum is analyzed with reference to a superplastic behavior of the equal channel angular pressing processed alloys.