Papers by Author: Sumio Sugiyama

Abstract: Owing to the phase segregation occurred during semisolid process, the ferroalloys products manufactured by semisolid process always exhibit inhomogeneous microstructure and poor mechanical properties. In this study, the post heat treatments including quenching treatment and tempering treatment with various processing parameters were carried out to improve the quality of Cr-V-Mo steel (JIS SKD61, AISI H13, DIN 1.2344) which processed by RAP (recrystallization and partial melting) processed. The microstructural characteristics (phase transformation, morphology of carbides, and distribution of alloying elements) and mechanical properties (hardness, tensile strength, elongation, impact toughness, and resistance to high-temperature wear) of specimens processed by RAP and heat treatments under various experimental conditions were investigated experimentally. Being quenched from 1050 °C after isothermal holding for 480 s and then tempered twice at 560 °C for 2 h, the microstructural evolution took placed in both former solid-phase and liquid-phase regions of the RAP-processed Cr-V-Mo steel specimen. During this post heat treatment strategy, the weakening of phase segregation, the redistribution of carbides, and the release of residual stress occurred and resulted in the improvement of microstructure and a good combination of mechanical properties.

Abstract: The feasibility of recycling machining grindings of aluminum alloys by semisolid process has been investigated. Machining grindings of A2011 aluminum alloy produced experimentally by lathe machining were used. The material is put into a metal mold and compressed up to 90 % of the true density at room temperature. The metal mold with the compressed machining grindings is heated up to a specified temperature. Afterwards, the metal mold is set into the extrusion container, and extrusion in hot and semisolid range was carried out. In this experimental study, extrusion load, internal structure of the product and mechanical properties (tensile strength, elongation, hardness) of the product are assessed. It was proven that semisolid extrusion is about 40% less extrusion load compared with that of hot extrusion, the shape of the machining grindings remained in the hot extrusion and the semisolid extrusion products extrusion ratios higher than 10 have excellent elongation property, which is comparable to the commercialized product.

Abstract: Thixoforming or Semi-Solid Metal Forming offers many advantages in comparison with casting and conventional forging. The purpose of the present study is to provide the basic microstructure and deformation data for austenitic and ferritic stainless steel under mushy state. As well known, the stainless steels solidify in different modes according to the different chemical compositions. In this paper, microstructural evolution of austenitic stainless steel type 304 which solidifies in FA mode ( L → L +δ → L +δ +γ →δ +γ →γ ),austenitic stainless steel type 310S which solidifies in A mode ( L → L +γ →γ ), and ferritic stainless steel type 430 which solidifies in F mode ( L → L +δ →δ )
are investigated during partial remelting by way of SIMA (Strain Induced Melted Activation). The results show that A and F mode of stainless steels melt directly at the grain boundary without phase transformation during reheating. A banded structure, originating from the primary dendritic segregation of the original ingots, is observed in type 310S steel during further heating. On the other hand, a perfect globular and insegregative two-phase semi-solid structure L +δ can be obtained while heated beyond the banded three-phase L +δ +γ semi-solid state in FA mode austenitic stainless steel type 304. This spheroidization can be attributed to the peritectic reaction occurred in the L +δ +γ semi-solid state. In addition, simple compression tests of these alloys in semi-solid state for varied combination of deformation rate and deformation temperature are conducted to examine the deformation behavior of stainless steel. Flow stress curves exhibit abrupt change in various alloys, even though in the same alloy such as type 304, various flow stresses are observed according to the difference in inner microstructure or morphology. Stress of type 310S steel shows the most reduction as the deformation temperature increasing at the same strain rate condition. The Liquid is centralized to periphery by the compression force in all deformed test pieces. Fracture, observed in all alloys except type 304 steel in globular L +δ semi-solid state, should be resulted from the lack of liquid in L +δ +γ state of type 304 steel and solidification crack in type 310S and type 430 steel. Deformation of solid particles occurs only in L +δ +γ state of type 304 steel. Last in this paper, various deformation mechanisms are proposed for various microstructures.

Abstract: The structural changes of the wrought magnesium alloy AZ31B in semisolid state were clarified using optical microscopy and hot-stage microscopy. The influence of heat treatment variables was assessed. Compression tests covering a range from room temperature to 673 K were carried out for mechanical property assessment; flow stress and breaking strain were determined. The following are the results: (1) The grain growth of the hot-extruded AZ31B without preprocessing sensitively reacted at temperature and retention time. (2) The hot-extruded AZ31B with 30 % preprocessing showed an almost perfectly spheroidized structure in a semisolid state under certain conditions. (3) Heating velocity markedly affected the spheroidizing rate of grains. (4) From the direct observation of the hot-extruded alloy AZ31B by hot-stage microscopy, spheroidization was observed in some crystal populations. (5) Spheroided materials in the semisolid temperature range had a lower flow stress and a larger breaking strain than nonspheroidized materials. These results indicate the possibility of manufacturing wrought magnesium alloy by cold working.