Papers by Author: T. Mori

Abstract: Single crystals of AlMgB ₁₄ and AlMgB ₂₂ were grown from a high-temperature aluminum metal flux in an Ar atmosphere. The optimum conditions for growing AlMgB ₂₂ and AlMgB ₁₄ were established using the starting mixtures of B/Mg=0.5-1.0 and B/Mg=2.0-6.0. The AlMgB ₁₄ and AlMgB ₂₂ crystals obtained have well-developed {001} and {100} faces, and were black with a metallic luster. The maximum dimensions of these crystals were about 5.2 mm and 4.6 mm, respectively. The values of micro-Vickers hardness of the AlMgB ₁₄ and AlMgB ₂₂ crystals are in the ranges of 23.9±0.6-27.6±0.6 GPa. The oxidation process of AlMgB ₁₄ and AlMgB ₂₂ crystals were studied up to 1473 K by TG-DTA method. The susceptibility of AlMgB14 with an increase at low temperatures does not show any particular features, being indicative of a paramagnetic contribution, which is likely due to impurities. The susceptibility of the AlMgB ₂₂ sample shows no apparent contribution from impurities and also does not have any anomalous behavior.