Authors: Vil D. Sitdikov, Igor V. Alexandrov, Jan T. Bonarski
Abstract: This paper presents the results of experimental X-ray structural analyses of both the evolution structure and the crystallographic one in the volume of Ti samples, subjected to the Severe Plastic Deformation (SPD), realized by torsion under high pressure equal to 6 GPa at temperature 298 K. The investigations have been carried out on the disk-shaped samples with the radius of 20 mm in an initial state (the as-received state) and in the states after 0.1, 0.5, 1 and 5 rotations by High-Pressure Torsion (HPT). In the result the evolution mechanisms of the general X-ray patterns, the volume fraction of phases, the character of preferred orientations, as well as the activity of various slip and twinning systems in α- and ω-phases, depending on the SPD degree have been found out. The received results allow explaining and forecasting the behavior of nanostructured Ti, considering the parameters of its microstructure and crystallographic texture.
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Authors: Jan T. Bonarski, Igor V. Alexandrov, Vil D. Sitdikov, Leszek Tarkowski, J. Grzonka, M. Bieda-Niemiec
Abstract: The common feature of the technologies, such as the equal channel angular pressing (ECAP) is the use of a changeable deformation path, which changes the configuration (value and direction) of the acting forces that impose various directions of plastic flow. The changes destabilize a temporary dislocation structure as well as the spatial distribution of the areas with elevated elastic energy cumulated in deformed lattice.
The application of that technique results in a potentially large deformation (up to several hundred percent) and plasticity of materials considered to be brittle at ambient temperature. The microstructure effects accompanied with intensive and large deformation are reflected in the space orientation of grains (crystallographic texture) as well as in the configuration of the residual stresses existing in deformed material.
The presented results based on experimental data registered by X-ray diffraction and TEM techniques are helpful in interpreting deformation mechanisms operating in the bend-zone of the ECAP tool during processing Ti-ingot by the mentioned method of severe plastic deformation.
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Authors: Igor V. Alexandrov, Vil D. Sitdikov
Abstract: In this article we present the results of the experimental research and those of the
processes developing the crystallographic texture of computer modeling in CP Ti in the process of
1-4 equal channel angular pressing (ECAP) passes along the route ВС. The goal of the research was
to determine the active deformation mechanisms, depending on the strain degree, accumulated in
the ECAP process. The research was carried out by the method of X-ray analysis and by computer
modeling. Computer modeling was carried out on the example of visco-plastic self-consistent
model. Thereby, the basal, the prismatic and the pyramidal (of the 1st and of the 2nd order) slip
systems were considered as possible active slip systems. Besides, the possibility of activating the
tensile and the compressive twinning systems were taken into consideration. As the result of the
carried out experimental research, the objective laws of forming preferred orientations were
determined. For the first time, with the help of computer modeling, made up to the 4th ECAP pass, it
was shown that the crystallographic texture development processes in CP Ti in ECAP, realized at
temperature of 723 K, can be explained by activation of the basal, prismatic and pyramidal (of the
1st order) slip systems and compressive twinning systems. Therefore, the increase of the ECAP
passes can lead to amplification of contribution of the basal and prismatic slip systems, as well as
the insignificant weakening of the contribution of pyramidal slip systems (of the 1st order).
Moreover, the compressive twinning can become obvious only in the 1st ECAP pass.
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Authors: Vil D. Sitdikov, Roza G. Chembarisova, Igor V. Alexandrov
Abstract: In the investigation the 3D version of the Estrin-Tóth dislocation model was used to
analyze deformation behaviour of pure Cu, subjected to high pressure torsion (HPT) under
pressures equal to 0.8, 2, 5, 8 GPa. As a result of the computer simulation, the nature and reasons
for strain hardening are analyzed, the dislocation density evolution versus degree of SPD and graincell
size versus degree of SPD curves were plotted. It is shown that the model adequately reflects
the acting deformation mechanisms and structural changes during HPT at different applied
pressures. It has been stated that an increase of the applied pressure at HPT leads to an increase in
the activity of dislocation sources and sinks in the grain-cell walls. Misorientations between
boundaries are estimated. It is revealed that an increase of the applied pressure contributes to a
growth of the misorientation angles between neighbouring grain-cells.
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